4-Amino-1-<2-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-1H-pyrrolo<2,3-b>pyridine

Base Information

• Chemical Name: 4-Amino-1-<2-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-1H-pyrrolo<2,3-b>pyridine
• CAS No.: 136859-72-8
• Molecular Formula: C₂₈H₃₃N₃O₃Si
• Molecular Weight: 487.674

Synonyms:4-Amino-1-<2-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-1H-pyrrolo<2,3-b>pyridine

Chemical Property of 4-Amino-1-<2-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-1H-pyrrolo<2,3-b>pyridine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 4-Amino-1-<2-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-1H-pyrrolo<2,3-b>pyridine

There total 3 articles about 4-Amino-1-<2-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-1H-pyrrolo<2,3-b>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1-<2-Deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine (132062-45-4) → 4-Amino-1-<2-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-1H-pyrrolo<2,3-b>pyridine (136859-72-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 2h; under 760 Torr; Ambient temperature;

DOI:10.1002/hlca.19910740514

Reference yield:

1-(2-deoxy-β-D-erythro-pentofuranosyl)-4-nitro-1H-pyrrolo[2,3-b]pyridine (124469-62-1) → 4-Amino-1-<2-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-1H-pyrrolo<2,3-b>pyridine (136859-72-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / pyridine / 8 h / Ambient temperature

2: 89 percent / H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1002/hlca.19910740514

Reference yield:

tert-butylchlorodiphenylsilane (58479-61-1) → 4-Amino-1-<2-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-1H-pyrrolo<2,3-b>pyridine (136859-72-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / pyridine / 8 h / Ambient temperature

2: 89 percent / H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1002/hlca.19910740514

upstream raw materials:

1-<2-Deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine

1-(2-deoxy-β-D-erythro-pentofuranosyl)-4-nitro-1H-pyrrolo[2,3-b]pyridine

tert-butylchlorodiphenylsilane

Downstream raw materials:

4-Amino-1-<2-deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-3-O--β-D-erythro-pentofuranosyl>-1H-pyrrolo<2,3-b>pyridine

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