C₂₈H₂₄N₆O₇

Base Information

Chemical Name:C₂₈H₂₄N₆O₇
CAS No.:1309611-49-1
Molecular Formula:C₂₈H₂₄N₆O₇
Molecular Weight:556.535
Hs Code.:

C<sub>28</sub>H<sub>24</sub>N<sub>6</sub>O<sub>7</sub>

Synonyms:C₂₈H₂₄N₆O₇

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Chemical Property of C₂₈H₂₄N₆O₇

Chemical Property:

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Technology Process of C₂₈H₂₄N₆O₇

There total 23 articles about C₂₈H₂₄N₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5453-67-8
2,6-bis(methoxycarbonyl)pyridine

: 1309611-49-1
C₂₈H₂₄N₆O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide / methanol; water / 12 h / 20 °C

2.1: 4-methyl-morpholine; chloroformic acid ethyl ester / tetrahydrofuran; N,N-dimethyl-formamide / 0.25 h / -10 - -5 °C

2.2: -10 - -5 °C

2.3: 30 h / 120 °C

3.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 50 °C

4.1: 4-methyl-morpholine; chloroformic acid ethyl ester / tetrahydrofuran; N,N-dimethyl-formamide / 0.5 h / -10 - -5 °C

4.2: -10 - 90 °C

5.1: sodium hydroxide / 1,4-dioxane; water / 20 °C

6.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 2 h

7.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; triethylamine; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol2011083

Reference yield:

: 100377-55-7
6-amino-4-methoxy-pyridine-2-carboxylic acid methyl ester

: C₂₀H₁₅ClN₄O₄

: 1309611-49-1
C₂₈H₂₄N₆O₇

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol2011083

Reference yield:

: 1262043-88-8
methyl 6-(benzyloxycarbonylamino)-pyridine-2-carboxylate

: 1309611-49-1
C₂₈H₂₄N₆O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 50 °C

2.1: 4-methyl-morpholine; chloroformic acid ethyl ester / tetrahydrofuran; N,N-dimethyl-formamide / 0.5 h / -10 - -5 °C

2.2: -10 - 90 °C

3.1: sodium hydroxide / 1,4-dioxane; water / 20 °C

4.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 2 h

5.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol2011083