(+)-(3R,5S)-diphenylcarbamic acid 2'-acetylamino-9'-{4-[dimethyl-(1,1,2-trimethylpropyl)-silanyloxymethyl]-3-formyl-cyclopent-2-enyl}-9H-purin-6'-yl ester

Base Information

Chemical Name:(+)-(3R,5S)-diphenylcarbamic acid 2'-acetylamino-9'-{4-[dimethyl-(1,1,2-trimethylpropyl)-silanyloxymethyl]-3-formyl-cyclopent-2-enyl}-9H-purin-6'-yl ester
CAS No.:737004-02-3
Molecular Formula:C₃₅H₄₂N₆O₅Si
Molecular Weight:654.841
Hs Code.:

(+)-(3R,5S)-diphenylcarbamic acid 2'-acetylamino-9'-{4-[dimethyl-(1,1,2-trimethylpropyl)-silanyloxymethyl]-3-formyl-cyclopent-2-enyl}-9H-purin-6'-yl ester

Synonyms:(+)-(3R,5S)-diphenylcarbamic acid 2'-acetylamino-9'-{4-[dimethyl-(1,1,2-trimethylpropyl)-silanyloxymethyl]-3-formyl-cyclopent-2-enyl}-9H-purin-6'-yl ester

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Chemical Property of (+)-(3R,5S)-diphenylcarbamic acid 2'-acetylamino-9'-{4-[dimethyl-(1,1,2-trimethylpropyl)-silanyloxymethyl]-3-formyl-cyclopent-2-enyl}-9H-purin-6'-yl ester

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Technology Process of (+)-(3R,5S)-diphenylcarbamic acid 2'-acetylamino-9'-{4-[dimethyl-(1,1,2-trimethylpropyl)-silanyloxymethyl]-3-formyl-cyclopent-2-enyl}-9H-purin-6'-yl ester

There total 1 articles about (+)-(3R,5S)-diphenylcarbamic acid 2'-acetylamino-9'-{4-[dimethyl-(1,1,2-trimethylpropyl)-silanyloxymethyl]-3-formyl-cyclopent-2-enyl}-9H-purin-6'-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Diphenyl-carbamic acid 2-acetylamino-9-((1R,4S)-3-formyl-4-hydroxymethyl-cyclopent-2-enyl)-9H-purin-6-yl ester

: 67373-56-2
chlorodimethyl(1,1,2-trimethylpropyl)silane

: 737004-02-3
(+)-(3R,5S)-diphenylcarbamic acid 2'-acetylamino-9'-{4-[dimethyl-(1,1,2-trimethylpropyl)-silanyloxymethyl]-3-formyl-cyclopent-2-enyl}-9H-purin-6'-yl ester

Guidance literature:: With pyridine; at 20 ℃; for 16h;
DOI:10.1002/chem.200400079

Reference yield:

: 737004-02-3
(+)-(3R,5S)-diphenylcarbamic acid 2'-acetylamino-9'-{4-[dimethyl-(1,1,2-trimethylpropyl)-silanyloxymethyl]-3-formyl-cyclopent-2-enyl}-9H-purin-6'-yl ester

: 737004-19-2
(-)-(1'R,4'S)-4-amino-9-{4'-[dimethyl-(1,1,2-trimethylpropyl)-silanyloxymethyl]-3'-hydroxymethyl-cyclopent-2'-enyl}-1,9-dihydro-purin-6-one

: Diphenyl-carbamic acid 2-acetylamino-9-{(1R,4S)-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxymethyl]-3-hydroxymethyl-cyclopent-2-enyl}-9H-purin-6-yl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at -78 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1002/chem.200400079