1-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>-2-<4-(3-bromomethylphenoxy)-3-methoxyphenyl>ethane

Base Information

Chemical Name:1-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>-2-<4-(3-bromomethylphenoxy)-3-methoxyphenyl>ethane
CAS No.:103561-08-6
Molecular Formula:C₃₀H₂₈Br₂O₄
Molecular Weight:612.358
Hs Code.:

Synonyms:1-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>-2-<4-(3-bromomethylphenoxy)-3-methoxyphenyl>ethane

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Chemical Property of 1-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>-2-<4-(3-bromomethylphenoxy)-3-methoxyphenyl>ethane

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Technology Process of 1-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>-2-<4-(3-bromomethylphenoxy)-3-methoxyphenyl>ethane

There total 12 articles about 1-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>-2-<4-(3-bromomethylphenoxy)-3-methoxyphenyl>ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 103561-05-3
1-<3-(4-hydroxymethylphenoxy)-4-methoxyphenyl>-2-<4-(3-hydroxymethylphenoxy)-3-methoxyphenyl>ethane

: 103561-08-6
1-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>-2-<4-(3-bromomethylphenoxy)-3-methoxyphenyl>ethane

Guidance literature:: With phosphorus tribromide; In benzene; at 80 ℃; for 1h;

Reference yield:

: 621-59-0
isovanillin

: 103561-08-6
1-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>-2-<4-(3-bromomethylphenoxy)-3-methoxyphenyl>ethane

Guidance literature:: Multi-step reaction with 8 steps

1: 96 percent / NH₄NO₃ / ethanol / 24 h

2: 30 percent / K₂CO₃, CuO / pyridine / 48 h / Heating

3: 90 percent / NaBH₄ / ethanol / 1 h

4: 47percent HBr / benzene; H₂O / 1 h

5: 76 percent / acetonitrile / 1 h / Heating

6: 1) NaOMe, 2) H₂ / 2) palladium-charcoal / 1) methanol, 1h, 2) ethyl acetate, ethanol

7: 87 percent / LiAlH₄ / tetrahydrofuran / 1 h

8: 100 percent / PBr₃ / benzene / 1 h / 80 °C

With ammonium nitrate; sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen bromide; hydrogen; sodium methylate; phosphorus tribromide; potassium carbonate; copper(II) oxide; palladium on activated charcoal; In tetrahydrofuran; pyridine; ethanol; water; acetonitrile; benzene;

Reference yield:

: 619-42-1
4-methoxycarbonylphenyl bromide

: 103561-08-6
1-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>-2-<4-(3-bromomethylphenoxy)-3-methoxyphenyl>ethane

Guidance literature:: Multi-step reaction with 7 steps

1: 30 percent / K₂CO₃, CuO / pyridine / 48 h / Heating

2: 90 percent / NaBH₄ / ethanol / 1 h

3: 47percent HBr / benzene; H₂O / 1 h

4: 76 percent / acetonitrile / 1 h / Heating

5: 1) NaOMe, 2) H₂ / 2) palladium-charcoal / 1) methanol, 1h, 2) ethyl acetate, ethanol

6: 87 percent / LiAlH₄ / tetrahydrofuran / 1 h

7: 100 percent / PBr₃ / benzene / 1 h / 80 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen bromide; hydrogen; sodium methylate; phosphorus tribromide; potassium carbonate; copper(II) oxide; palladium on activated charcoal; In tetrahydrofuran; pyridine; ethanol; water; acetonitrile; benzene;