C₂₅H₂₆N₂O₅

Base Information

• Chemical Name: C₂₅H₂₆N₂O₅
• CAS No.: 929211-74-5
• Molecular Formula: C₂₅H₂₆N₂O₅
• Molecular Weight: 434.492
• Mol file: 929211-74-5.mol

Synonyms:C₂₅H₂₆N₂O₅

Chemical Property of C₂₅H₂₆N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₂₆N₂O₅

There total 13 articles about C₂₅H₂₆N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C27H25F3N2O6 (722499-82-3) → C25H26N2O5 (929211-74-5)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1248/cpb.54.1662

Reference yield:

[3,5-bis(benzyloxy)-4-methoxyphenyl]methanol (27229-56-7) → C25H26N2O5 (929211-74-5)

Guidance literature:

Multi-step reaction with 7 steps

1.1: 96 percent / pyridinium chlorochromate / tetrahydrofuran / 3 h / 20 °C

2.1: dioxane / 24 h / 20 °C

2.2: 64 percent / HCl / dioxane / 24 h / 20 °C

3.1: 94 percent / pyridine / 0.25 h / 0 °C

4.1: 61 percent / phenyliodine(III) bis(trifluoroacetate) / 2,2,2-trifluoro-ethanol / 0.17 h / -40 °C

5.1: 95 percent / BCl₃ / CH₂Cl₂ / 20 h / -78 °C

6.1: 92 percent / lithium tri-sec-butylborohydride / tetrahydrofuran / 24 h / -78 °C

7.1: 100 percent / aq. NaOH / tetrahydrofuran / 12 h / 20 °C

With pyridine; sodium hydroxide; boron trichloride; L-Selectride; pyridinium chlorochromate; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; 1,4-dioxane; dichloromethane; 2,2,2-trifluoroethanol; 5.1: Michael addition;

DOI:10.1248/cpb.54.1662

Reference yield:

methyl galloate (99-24-1) → C25H26N2O5 (929211-74-5)

Guidance literature:

Multi-step reaction with 10 steps

1.1: K₂CO₃ / dimethylformamide / 1 h / 85 °C

1.2: 76 percent / dimethylformamide / 24 h / 20 °C

2.1: 95 percent / K₂CO₃ / dimethylformamide / 1.5 h / 150 °C

3.1: 96 percent / lithium aluminum hydride / tetrahydrofuran / 3 h / 60 °C

4.1: 96 percent / pyridinium chlorochromate / tetrahydrofuran / 3 h / 20 °C

5.1: dioxane / 24 h / 20 °C

5.2: 64 percent / HCl / dioxane / 24 h / 20 °C

6.1: 94 percent / pyridine / 0.25 h / 0 °C

7.1: 61 percent / phenyliodine(III) bis(trifluoroacetate) / 2,2,2-trifluoro-ethanol / 0.17 h / -40 °C

8.1: 95 percent / BCl₃ / CH₂Cl₂ / 20 h / -78 °C

9.1: 92 percent / lithium tri-sec-butylborohydride / tetrahydrofuran / 24 h / -78 °C

10.1: 100 percent / aq. NaOH / tetrahydrofuran / 12 h / 20 °C

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; boron trichloride; L-Selectride; potassium carbonate; pyridinium chlorochromate; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; 1,4-dioxane; dichloromethane; 2,2,2-trifluoroethanol; N,N-dimethyl-formamide; 8.1: Michael addition;

DOI:10.1248/cpb.54.1662

upstream raw materials:

C₂₇H₂₅F₃N₂O₆

[3,5-bis(benzyloxy)-4-methoxyphenyl]methanol

methyl galloate

3,5-bis(benzyloxy)-4-methoxybenzaldehyde

Refernces