3-[1-methyl-2(RS_S)-phenylsulfinyl-(1S)-ethyl]-(2S,3R)-oxiran-2-ylmethanol

Base Information

Chemical Name:3-[1-methyl-2(RS_S)-phenylsulfinyl-(1S)-ethyl]-(2S,3R)-oxiran-2-ylmethanol
CAS No.:689283-23-6
Molecular Formula:C₁₂H₁₆O₃S
Molecular Weight:240.323
Hs Code.:

3-[1-methyl-2(RS<sub>S</sub>)-phenylsulfinyl-(1S)-ethyl]-(2S,3R)-oxiran-2-ylmethanol

Synonyms:3-[1-methyl-2(RS_S)-phenylsulfinyl-(1S)-ethyl]-(2S,3R)-oxiran-2-ylmethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[1-methyl-2(RS_S)-phenylsulfinyl-(1S)-ethyl]-(2S,3R)-oxiran-2-ylmethanol

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Technology Process of 3-[1-methyl-2(RS_S)-phenylsulfinyl-(1S)-ethyl]-(2S,3R)-oxiran-2-ylmethanol

There total 2 articles about 3-[1-methyl-2(RS_S)-phenylsulfinyl-(1S)-ethyl]-(2S,3R)-oxiran-2-ylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 689283-22-5
2-tert-butyldiphenylsilyloxymethyl-3-[1-methyl-2(RS_S)-phenylsulfinyl-(1S)-ethyl]-(2S,3R)-oxirane

: 689283-23-6
3-[1-methyl-2(RS_S)-phenylsulfinyl-(1S)-ethyl]-(2S,3R)-oxiran-2-ylmethanol

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1016/j.tet.2004.01.088

Reference yield:

: 628340-18-1
2-bromo-1-tert-butyldiphenylsilyloxy-4-methyl-5(RS_S)-phenylsulfinyl-(2R,3R,4S)-pentan-3-ol

: 689283-23-6
3-[1-methyl-2(RS_S)-phenylsulfinyl-(1S)-ethyl]-(2S,3R)-oxiran-2-ylmethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / K₂CO₃ / methanol / 0 - 20 °C

2: 90 percent / acetic acid; tetrabutylammonium fluoride / tetrahydrofuran / 2 h / 0 °C

With tetrabutyl ammonium fluoride; potassium carbonate; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1016/j.tet.2004.01.088