(2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol

Base Information

Chemical Name:(2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol
CAS No.:849479-34-1
Molecular Formula:C₁₄H₂₀O₄S
Molecular Weight:284.376
Hs Code.:

Synonyms:(2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol

Suppliers and Price of (2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol

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Technology Process of (2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol

There total 1 articles about (2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 94958-32-4
tert-Butyl-((2S,3S,4R,5R,6S)-3,5-dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-yloxy)-dimethyl-silane

: 849479-34-1
(2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 4h;
DOI:10.1002/anie.200462267

Reference yield: 99.0%

: 849479-34-1
(2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol

: 3019-71-4
Trichloroacetyl isocyanate

: 849479-36-3
Carbamic acid (2S,3S,4R,5R,6S)-3,5-dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester

Guidance literature:: (2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol; Trichloroacetyl isocyanate; In dichloromethane; at 20 ℃; for 1h;

With potassium carbonate; In methanol; at 20 ℃; for 2h;
DOI:10.1002/anie.200462267

Reference yield: 84.0%

: 849479-34-1
(2S,3R,4R,5R,6S)-3,5-Dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-ol

: 94958-16-4
tert-Butyl-((2S,3R,4R,5S,6S)-2-fluoro-3,5-dimethoxy-6-methyl-tetrahydro-pyran-4-yloxy)-dimethyl-silane

: 849479-35-2
tert-Butyl-[(2S,3R,4R,5S,6S)-2-((2S,3S,4R,5R,6S)-3,5-dimethoxy-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-4-yloxy)-3,5-dimethoxy-6-methyl-tetrahydro-pyran-4-yloxy]-dimethyl-silane

Guidance literature:: With 4 A molecular sieve; silver perchlorate; tin(ll) chloride; In diethyl ether; at 0 - 20 ℃; for 4h;
DOI:10.1002/anie.200462267