Technology Process of C20H19NO4
There total 3 articles about C20H19NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
pyridine;
In
isopropyl alcohol;
at 80 - 82 ℃;
for 8h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Cumene hydroperoxide / titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 48 h / -35 °C / Molecular sieve
2: sodium hydride / tetra-(n-butyl)ammonium iodide / tetrahydrofuran; mineral oil / -15 - 20 °C / Inert atmosphere
3: pyridine / isopropyl alcohol / 8 h / 80 - 82 °C
With
Cumene hydroperoxide; sodium hydride;
pyridine; titanium(IV) isopropylate; L-(+)-diisopropyl tartrate; tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; dichloromethane; isopropyl alcohol; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride / tetra-(n-butyl)ammonium iodide / tetrahydrofuran; mineral oil / -15 - 20 °C / Inert atmosphere
2: pyridine / isopropyl alcohol / 8 h / 80 - 82 °C
With
sodium hydride;
pyridine; tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; isopropyl alcohol; mineral oil;