N,N',N''-tris-(brommethylboryl)-B,B',B''-trimethylborazine

Base Information

Chemical Name:N,N',N''-tris-(brommethylboryl)-B,B',B''-trimethylborazine
CAS No.:98885-56-4
Molecular Formula:C₆H₁₈B₆Br₃N₃
Molecular Weight:436.807
Hs Code.:

Synonyms:N,N',N''-tris-(brommethylboryl)-B,B',B''-trimethylborazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N',N''-tris-(brommethylboryl)-B,B',B''-trimethylborazine

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Technology Process of N,N',N''-tris-(brommethylboryl)-B,B',B''-trimethylborazine

There total 1 articles about N,N',N''-tris-(brommethylboryl)-B,B',B''-trimethylborazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 17933-16-3
dibromomethylborane

: 1068-70-8
tris(trimethylstannyl)amine

: 98906-22-0
tris-(brommethylboryl)amine

: 98885-56-4
N,N',N''-tris-(brommethylboryl)-B,B',B''-trimethylborazine

: 1066-44-0
trimethyltin bromide

Guidance literature:: In dichloromethane; byproducts: Me2SnBr2; an excess of a soln. of MeBBr2 was added to a soln. of the amine, both in CH2Cl2, at -60°C with stirring and warmed up to room temp.; all reactions under N2 with exclusion of moisture;; evapn. of volatiles at 100 Torr; distn. yielded Me3SnBr (50°C/ 5 Torr) and product (76°C/4 Torr); redistn. (40°C/3 Torr) yielded a product with ca. 3% Me2SnBr2; residue yielded 2 nd. product (144 °C/0.01 Torr); elem.anal.;;