3-N-benzoyl-3',5'-di-O-benzoyl-5-(3-tert-butyldimethylsilyloxypropyl)-2'-deoxyuridine

Base Information

Chemical Name:3-N-benzoyl-3',5'-di-O-benzoyl-5-(3-tert-butyldimethylsilyloxypropyl)-2'-deoxyuridine
CAS No.:1037176-25-2
Molecular Formula:C₃₉H₄₄N₂O₉Si
Molecular Weight:712.872
Hs Code.:

Synonyms:3-N-benzoyl-3',5'-di-O-benzoyl-5-(3-tert-butyldimethylsilyloxypropyl)-2'-deoxyuridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-N-benzoyl-3',5'-di-O-benzoyl-5-(3-tert-butyldimethylsilyloxypropyl)-2'-deoxyuridine

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Technology Process of 3-N-benzoyl-3',5'-di-O-benzoyl-5-(3-tert-butyldimethylsilyloxypropyl)-2'-deoxyuridine

There total 1 articles about 3-N-benzoyl-3',5'-di-O-benzoyl-5-(3-tert-butyldimethylsilyloxypropyl)-2'-deoxyuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 89031-84-5
3-(tert-butyldimethylsilyloxy)propyl bromide

: 156897-72-2
3-N-benzoyl-3',5'-di-O-benzoyl-5-iodo-2'-deoxyuridine

: 1037176-25-2
3-N-benzoyl-3',5'-di-O-benzoyl-5-(3-tert-butyldimethylsilyloxypropyl)-2'-deoxyuridine

Guidance literature:: 3-(tert-butyldimethylsilyloxy)propyl bromide; With iodine; zinc; In N,N-dimethyl acetamide; at 80 ℃; Inert atmosphere;

3-N-benzoyl-3',5'-di-O-benzoyl-5-iodo-2'-deoxyuridine; With bis(tri-t-butylphosphine)palladium⁽⁰⁾; In N,N-dimethyl acetamide; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jm800501d