[osmium(2,2'-bipyridine)2(3-(pyrrol-1-yl-methyl)pyridine)Cl]PF₆

Base Information

• Chemical Name: [osmium(2,2'-bipyridine)2(3-(pyrrol-1-yl-methyl)pyridine)Cl]PF₆
• CAS No.: 1024934-58-4
• Molecular Formula: C₃₀H₂₆ClN₆Os*F₆P
• Molecular Weight: 841.194
• Mol file: 1024934-58-4.mol

Synonyms:[osmium(2,2'-bipyridine)2(3-(pyrrol-1-yl-methyl)pyridine)Cl]PF₆

Chemical Property of [osmium(2,2'-bipyridine)2(3-(pyrrol-1-yl-methyl)pyridine)Cl]PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of [osmium(2,2'-bipyridine)2(3-(pyrrol-1-yl-methyl)pyridine)Cl]PF₆

There total 1 articles about [osmium(2,2'-bipyridine)2(3-(pyrrol-1-yl-methyl)pyridine)Cl]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

ammonium hexafluorophosphate + bis(2,2'-bipyridine)osmium(II) dichloride (15702-72-4,79982-56-2) + 3-((1H-pyrrol-1-yl)methyl)pyridine (80866-95-1) → [osmium(2,2'-bipyridine)2(3-(pyrrol-1-yl-methyl)pyridine)Cl]PF6 (1024934-58-4)

Guidance literature:

In ethylene glycol; stirred in dark for 20 min; heated to reflux temp. for 30 min; allowed to cool to room temp.; filtered; excess of NH4PF6 added; placed at 4°C for 30-60 min; pptd.; dried under vac.; recrystd. (acetone/water); filtered; washed (water); dried overnight in vac. oven at 60°C, 200 mbar pressure;

DOI:10.1016/j.electacta.2008.01.049

upstream raw materials:

bis(2,2'-bipyridine)osmium(II) dichloride

3-((1H-pyrrol-1-yl)methyl)pyridine