trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-3-(1'''-methyl-1'''-phenylselenoethyl)-2-methylpent-1-en-3-ol

Base Information

Chemical Name:trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-3-(1'''-methyl-1'''-phenylselenoethyl)-2-methylpent-1-en-3-ol
CAS No.:115842-84-7
Molecular Formula:C₃₁H₅₂O₂SeSi
Molecular Weight:563.798
Hs Code.:

Synonyms:trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-3-(1'''-methyl-1'''-phenylselenoethyl)-2-methylpent-1-en-3-ol

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Chemical Property of trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-3-(1'''-methyl-1'''-phenylselenoethyl)-2-methylpent-1-en-3-ol

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Technology Process of trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-3-(1'''-methyl-1'''-phenylselenoethyl)-2-methylpent-1-en-3-ol

There total 5 articles about trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-3-(1'''-methyl-1'''-phenylselenoethyl)-2-methylpent-1-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 35446-87-8
2,2-bis (phenylseleno)propane

: 115842-83-6
trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-2-methylpent-1-en-3-one

: 115842-84-7
trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-3-(1'''-methyl-1'''-phenylselenoethyl)-2-methylpent-1-en-3-ol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; -78 deg C, 1 h, room temperature, 1 h;

Reference yield:

: 645-96-5
Benzeneselenol

: 115842-84-7
trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-3-(1'''-methyl-1'''-phenylselenoethyl)-2-methylpent-1-en-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / HCl gas / 0.5 h / 0 °C

2: 85 percent / butyl-lithium / tetrahydrofuran / -78 deg C, 1 h, room temperature, 1 h

With hydrogenchloride; n-butyllithium; In tetrahydrofuran;

Reference yield:

: 109263-23-2,115889-37-7
3-{(1R,2S)-2-[1-(tert-Butyl-dimethyl-silanyloxy)-allyl]-1-methyl-cyclohexyl}-propionaldehyde

: 115842-84-7
trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-3-(1'''-methyl-1'''-phenylselenoethyl)-2-methylpent-1-en-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / tetrahydrofuran / 0.5 h / Ambient temperature

2: 74 percent / chromium trioxide, pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 85 percent / butyl-lithium / tetrahydrofuran / -78 deg C, 1 h, room temperature, 1 h

With pyridine; chromium(VI) oxide; n-butyllithium; In tetrahydrofuran; dichloromethane;