Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-methyl-1-((2S,5R)-5-methyl-6-oxo-tetrahydro-pyran-2-yl)-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester

Base Information

Chemical Name:Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-methyl-1-((2S,5R)-5-methyl-6-oxo-tetrahydro-pyran-2-yl)-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester
CAS No.:79733-57-6
Molecular Formula:C₂₈H₃₉Cl₃O₇
Molecular Weight:593.972
Hs Code.:

Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-methyl-1-((2S,5R)-5-methyl-6-oxo-tetrahydro-pyran-2-yl)-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester

Synonyms:Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-methyl-1-((2S,5R)-5-methyl-6-oxo-tetrahydro-pyran-2-yl)-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester

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Chemical Property of Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-methyl-1-((2S,5R)-5-methyl-6-oxo-tetrahydro-pyran-2-yl)-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester

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Technology Process of Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-methyl-1-((2S,5R)-5-methyl-6-oxo-tetrahydro-pyran-2-yl)-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester

There total 3 articles about Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-methyl-1-((2S,5R)-5-methyl-6-oxo-tetrahydro-pyran-2-yl)-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79698-78-5,79733-55-4
4-Benzenesulfinyl-6-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-2-methyl-hexan-3-ol

: 79733-57-6
Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-methyl-1-((2S,5R)-5-methyl-6-oxo-tetrahydro-pyran-2-yl)-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Raney Ni, 2.) H₂ / 2.) Pd/C / 1.) hexane, 25 deg C, 2.) EtOAc

2: pyridine / 18 h / 25 °C

3: 1.) aq. HCl, 2.) PCC, NaOAc / 1.) THF, 25 deg C, 1 - 2 d, 2.) CH₂Cl₂, 25 deg C, 1 h

With hydrogenchloride; hydrogen; sodium acetate; nickel; pyridinium chlorochromate; palladium on activated charcoal; In pyridine;
DOI:10.1021/ja00410a056

Reference yield:

: 79698-79-6,79733-56-5
(S)-6-((2R,4S,5R)-4-Benzyloxy-5-methyl-tetrahydro-furan-2-yl)-2-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-2-methyl-hexan-3-ol

: 79733-57-6
Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-methyl-1-((2S,5R)-5-methyl-6-oxo-tetrahydro-pyran-2-yl)-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 18 h / 25 °C

2: 1.) aq. HCl, 2.) PCC, NaOAc / 1.) THF, 25 deg C, 1 - 2 d, 2.) CH₂Cl₂, 25 deg C, 1 h

With hydrogenchloride; sodium acetate; pyridinium chlorochromate; In pyridine;
DOI:10.1021/ja00410a056

Reference yield:

: 79698-80-9
Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-((2S,5R,6R)-6-tert-butoxy-5-methyl-tetrahydro-pyran-2-yl)-1-methyl-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester

: 79733-57-6
Carbonic acid (S)-4-((2R,4S,5R)-4-benzyloxy-5-methyl-tetrahydro-furan-2-yl)-1-[1-methyl-1-((2S,5R)-5-methyl-6-oxo-tetrahydro-pyran-2-yl)-ethyl]-butyl ester 2,2,2-trichloro-ethyl ester

Guidance literature:: With hydrogenchloride; sodium acetate; pyridinium chlorochromate; Multistep reaction; 1.) THF, 25 deg C, 1 - 2 d, 2.) CH₂Cl₂, 25 deg C, 1 h;
DOI:10.1021/ja00410a056