C₂₄H₂₄BrNO₇S

Base Information

Chemical Name:C₂₄H₂₄BrNO₇S
CAS No.:1094172-69-6
Molecular Formula:C₂₄H₂₄BrNO₇S
Molecular Weight:550.427
Hs Code.:

C<sub>24</sub>H<sub>24</sub>BrNO<sub>7</sub>S

Synonyms:C₂₄H₂₄BrNO₇S

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Chemical Property of C₂₄H₂₄BrNO₇S

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Technology Process of C₂₄H₂₄BrNO₇S

There total 8 articles about C₂₄H₂₄BrNO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1333378-28-1
C₂₄H₂₃NO₇S

: 1094172-69-6
C₂₄H₂₄BrNO₇S

Guidance literature:: With hydrogen bromide; acetic acid; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1002/ejoc.201100242

Reference yield:

: 1333378-25-8
C₂₁H₂₂BrNO₅S

: 1094172-69-6
C₂₄H₂₄BrNO₇S

Guidance literature:: Multi-step reaction with 5 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 1,4-dioxane / 21 h / 100 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.33 h / 0 °C

3: camphor-10-sulfonic acid / methanol / 2 h / 20 °C

4: pyridine; dmap / 12 h / 20 °C

5: hydrogen bromide; acetic acid / tetrahydrofuran / 0.5 h / 0 °C

With pyridine; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen bromide; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; water; 1: Sonogashira coupling;
DOI:10.1002/ejoc.201100242

Reference yield:

: 1333378-27-0
C₂₃H₂₃NO₅S

: 1094172-69-6
C₂₄H₂₄BrNO₇S

Guidance literature:: Multi-step reaction with 3 steps

1: camphor-10-sulfonic acid / methanol / 2 h / 20 °C

2: pyridine; dmap / 12 h / 20 °C

3: hydrogen bromide; acetic acid / tetrahydrofuran / 0.5 h / 0 °C

With pyridine; dmap; camphor-10-sulfonic acid; hydrogen bromide; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1002/ejoc.201100242