Carbamic acid, (2-hydroxy-2-oxiranylethyl)-, 1,1-dimethylethyl ester, [R-

Base Information

• Chemical Name: Carbamic acid, (2-hydroxy-2-oxiranylethyl)-, 1,1-dimethylethyl ester, [R-
• CAS No.: 153729-79-4
• Molecular Formula: C₉H₁₇NO₄
• Molecular Weight: 203.238
• Mol file: 153729-79-4.mol

Synonyms:Carbamicacid, (2-hydroxy-2-oxiranylethyl)-, 1,1-dimethylethyl ester, [R-(R*,R*)]- (9CI)

Chemical Property of Carbamic acid, (2-hydroxy-2-oxiranylethyl)-, 1,1-dimethylethyl ester, [R-

Chemical Property:

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Technology Process of Carbamic acid, (2-hydroxy-2-oxiranylethyl)-, 1,1-dimethylethyl ester, [R-

There total 2 articles about Carbamic acid, (2-hydroxy-2-oxiranylethyl)-, 1,1-dimethylethyl ester, [R- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-5-((S)-2-Chloro-1-hydroxy-ethyl)-2-oxo-oxazolidine-3-carboxylic acid tert-butyl ester → tert-butyl N-[(2R)-2-hydroxy-2-[(2R)-oxiran-2-yl]ethyl]carbamate (153729-79-4)

Guidance literature:

With potassium carbonate; In methanol; Yield given; Ambient temperature;

DOI:10.1016/S0040-4039(00)73877-9

Reference yield:

C14H24ClNO4 (121030-31-7) → tert-butyl N-[(2R)-2-hydroxy-2-[(2R)-oxiran-2-yl]ethyl]carbamate (153729-79-4)

Guidance literature:

Multi-step reaction with 2 steps

1: modified AD-mix-β / 2-methyl-propan-2-ol; H2O / 0 °C

2: K₂CO₃ / methanol / Ambient temperature

With modified AD-mix-β ; potassium carbonate; In methanol; water; tert-butyl alcohol;

DOI:10.1016/S0040-4039(00)73877-9

upstream raw materials:

C₁₄H₂₄ClNO₄

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