6-benzyl-4-[(dimethylamino)methyl]-3-styrylisoxazolo[3,4-d]pyridazin-7(6H)-one

Base Information

Chemical Name:6-benzyl-4-[(dimethylamino)methyl]-3-styrylisoxazolo[3,4-d]pyridazin-7(6H)-one
CAS No.:910316-52-8
Molecular Formula:C₂₃H₂₂N₄O₂
Molecular Weight:386.453
Hs Code.:

Synonyms:6-benzyl-4-[(dimethylamino)methyl]-3-styrylisoxazolo[3,4-d]pyridazin-7(6H)-one

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Chemical Property of 6-benzyl-4-[(dimethylamino)methyl]-3-styrylisoxazolo[3,4-d]pyridazin-7(6H)-one

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Technology Process of 6-benzyl-4-[(dimethylamino)methyl]-3-styrylisoxazolo[3,4-d]pyridazin-7(6H)-one

There total 5 articles about 6-benzyl-4-[(dimethylamino)methyl]-3-styrylisoxazolo[3,4-d]pyridazin-7(6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 910316-33-5
4-ethoxymethyl-3-methylisoxazolo[3,4-d]pyridazin-7(6H)-one

: 910316-52-8
6-benzyl-4-[(dimethylamino)methyl]-3-styrylisoxazolo[3,4-d]pyridazin-7(6H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: 48 percent / K₂CO₃ / dimethylformamide / Heating

2: 60 percent / HBr; AcOH / 8 h / 140 °C

3: 57 percent / K₂CO₃ / dimethylformamide / 2 h / 20 °C

4: 34 percent / CH₃ONa / methanol / Heating

With hydrogen bromide; sodium methylate; potassium carbonate; acetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm060265+

Reference yield:

: 910316-31-3
ethyl 4-ethoxymethylcarbonyl-5-methylisoxazole-3-carboxylate

: 910316-52-8
6-benzyl-4-[(dimethylamino)methyl]-3-styrylisoxazolo[3,4-d]pyridazin-7(6H)-one

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / hydrazine hydrate / ethanol / 20 °C

2: 48 percent / K₂CO₃ / dimethylformamide / Heating

3: 60 percent / HBr; AcOH / 8 h / 140 °C

4: 57 percent / K₂CO₃ / dimethylformamide / 2 h / 20 °C

5: 34 percent / CH₃ONa / methanol / Heating

With hydrogen bromide; sodium methylate; potassium carbonate; hydrazine hydrate; acetic acid; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm060265+

Reference yield:

: 910316-49-3
6-benzyl-4-bromomethyl-3-methylisoxazolo[3,4-d]pyridazin-7(6H)-one

: 910316-52-8
6-benzyl-4-[(dimethylamino)methyl]-3-styrylisoxazolo[3,4-d]pyridazin-7(6H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / K₂CO₃ / dimethylformamide / 2 h / 20 °C

2: 34 percent / CH₃ONa / methanol / Heating

With sodium methylate; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm060265+