1-methyl N-[2-(benzyloxy)-2-oxoethyl]-N-(tert-butoxycarbonyl)-L-aspartate

Base Information

Chemical Name:1-methyl N-[2-(benzyloxy)-2-oxoethyl]-N-(tert-butoxycarbonyl)-L-aspartate
CAS No.:1033713-01-7
Molecular Formula:C₁₉H₂₅NO₈
Molecular Weight:395.409
Hs Code.:

Synonyms:1-methyl N-[2-(benzyloxy)-2-oxoethyl]-N-(tert-butoxycarbonyl)-L-aspartate

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Chemical Property of 1-methyl N-[2-(benzyloxy)-2-oxoethyl]-N-(tert-butoxycarbonyl)-L-aspartate

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Technology Process of 1-methyl N-[2-(benzyloxy)-2-oxoethyl]-N-(tert-butoxycarbonyl)-L-aspartate

There total 1 articles about 1-methyl N-[2-(benzyloxy)-2-oxoethyl]-N-(tert-butoxycarbonyl)-L-aspartate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1033712-98-9
4-tert-Butyl 1-Methyl N-[2-(benzyloxy)-2-oxoethyl]-L-aspartate

: 1033713-01-7
1-methyl N-[2-(benzyloxy)-2-oxoethyl]-N-(tert-butoxycarbonyl)-L-aspartate

Guidance literature:: 4-tert-Butyl 1-Methyl N-[2-(benzyloxy)-2-oxoethyl]-L-aspartate; With water; trifluoroacetic acid; at -10 - 20 ℃; for 3h;

With sodium hydroxide; In water; pH=~ 3; Cooling with ice;

di-tert-butyl dicarbonate;

Reference yield: 25.0%

: 1033713-01-7
1-methyl N-[2-(benzyloxy)-2-oxoethyl]-N-(tert-butoxycarbonyl)-L-aspartate

: 100-51-6,185532-71-2
benzyl alcohol

: 1033713-05-1
Methyl 3-{[(Benzyloxy)carbonyl]amino}-N-[2-(benzyloxy)-2-oxoethyl]-N-(tert-butoxycarbonyl)-L-alaninate

Guidance literature:: 1-methyl N-[2-(benzyloxy)-2-oxoethyl]-N-(tert-butoxycarbonyl)-L-aspartate; With diphenyl phosphoryl azide; triethylamine; In benzene; at 20 ℃; for 1.5h; Reflux;

benzyl alcohol; In benzene; Reflux;