(3,4,6-tri-O-benzoyl-2-deoxy-1-thioureido-β-D-arabino-hexopyranosyl)pseudothiourea hydrobromide

Base Information

Chemical Name:(3,4,6-tri-O-benzoyl-2-deoxy-1-thioureido-β-D-arabino-hexopyranosyl)pseudothiourea hydrobromide
CAS No.:75744-90-0
Molecular Formula:BrH*C₂₈H₂₆N₂O₇S
Molecular Weight:615.502
Hs Code.:

Synonyms:(3,4,6-tri-O-benzoyl-2-deoxy-1-thioureido-β-D-arabino-hexopyranosyl)pseudothiourea hydrobromide

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Chemical Property of (3,4,6-tri-O-benzoyl-2-deoxy-1-thioureido-β-D-arabino-hexopyranosyl)pseudothiourea hydrobromide

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of (3,4,6-tri-O-benzoyl-2-deoxy-1-thioureido-β-D-arabino-hexopyranosyl)pseudothiourea hydrobromide

There total 2 articles about (3,4,6-tri-O-benzoyl-2-deoxy-1-thioureido-β-D-arabino-hexopyranosyl)pseudothiourea hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 17356-08-0
thiourea

: 51842-46-7
3,4,6-tri-O-benzoyl-2-deoxy-α-D-arabino-hexapyranosyl bromide

: 75744-90-0
(3,4,6-tri-O-benzoyl-2-deoxy-1-thioureido-β-D-arabino-hexopyranosyl)pseudothiourea hydrobromide

Guidance literature:: In acetone; for 1h; Heating;
DOI:10.1016/S0008-6215(00)85564-0

Reference yield:

: 16750-08-6
1,3,4,6-Tetra-O-benzoyl-2-deoxy-β-D-arabino-hexopyranose

: 75744-90-0
(3,4,6-tri-O-benzoyl-2-deoxy-1-thioureido-β-D-arabino-hexopyranosyl)pseudothiourea hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 49percent hydrobromic acid / CH₂Cl₂; H₂O / 0 - 5 °C

2: 95 percent / acetone / 1 h / Heating

With hydrogen bromide; In dichloromethane; water; acetone;
DOI:10.1016/S0008-6215(00)85564-0