1,5-bis(3-chloro-2,4,5,6-tetrafluorophenyl)-2,4-diaza-1,3,5-trithia-2,3-pentadiene

Base Information

Chemical Name:1,5-bis(3-chloro-2,4,5,6-tetrafluorophenyl)-2,4-diaza-1,3,5-trithia-2,3-pentadiene
CAS No.:1258866-40-8
Molecular Formula:C₁₂Cl₂F₈N₂S₃
Molecular Weight:491.237
Hs Code.:

Synonyms:1,5-bis(3-chloro-2,4,5,6-tetrafluorophenyl)-2,4-diaza-1,3,5-trithia-2,3-pentadiene

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Chemical Property of 1,5-bis(3-chloro-2,4,5,6-tetrafluorophenyl)-2,4-diaza-1,3,5-trithia-2,3-pentadiene

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Technology Process of 1,5-bis(3-chloro-2,4,5,6-tetrafluorophenyl)-2,4-diaza-1,3,5-trithia-2,3-pentadiene

There total 3 articles about 1,5-bis(3-chloro-2,4,5,6-tetrafluorophenyl)-2,4-diaza-1,3,5-trithia-2,3-pentadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1258626-43-5
3-chloro-2,4,5,6-tetrafluorophenylsulfenyl chloride

: 1258866-40-8
1,5-bis(3-chloro-2,4,5,6-tetrafluorophenyl)-2,4-diaza-1,3,5-trithia-2,3-pentadiene

Guidance literature:: With N,N'-bis(trimethylsilyl)sulfurdiimide; In hexane; for 1h; Inert atmosphere;
DOI:10.1002/ejic.201000607

Reference yield:

: 5172-06-5
1-chloro-2,3,4,6-tetrafluorobenzene

: 1258866-40-8
1,5-bis(3-chloro-2,4,5,6-tetrafluorophenyl)-2,4-diaza-1,3,5-trithia-2,3-pentadiene

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; hexane / 1.5 h / -60 °C / Inert atmosphere

1.2: -60 - 0 °C / Inert atmosphere

1.3: 0 °C

2.1: chlorine / tetrachloromethane

3.1: N,N'-bis(trimethylsilyl)sulfurdiimide / hexane / 1 h / Inert atmosphere

With n-butyllithium; N,N'-bis(trimethylsilyl)sulfurdiimide; chlorine; In tetrachloromethane; diethyl ether; hexane;
DOI:10.1002/ejic.201000607

Reference yield:

: 1258626-39-9
3,3-dichloro-2,2',4,4',5,5',6,6'-octafluorodiphenyl disulfide

: 1258866-40-8
1,5-bis(3-chloro-2,4,5,6-tetrafluorophenyl)-2,4-diaza-1,3,5-trithia-2,3-pentadiene

Guidance literature:: Multi-step reaction with 2 steps

1: chlorine / tetrachloromethane

2: N,N'-bis(trimethylsilyl)sulfurdiimide / hexane / 1 h / Inert atmosphere

With N,N'-bis(trimethylsilyl)sulfurdiimide; chlorine; In tetrachloromethane; hexane;
DOI:10.1002/ejic.201000607