2-but-3-enyl-3-chloro-4,6-dihydroxy-benzoic acid 2-(2-methoxy-3,6-bis-methoxymethoxy-5-nitro-phenyl)-1-methyl-ethyl ester

Base Information

Chemical Name:2-but-3-enyl-3-chloro-4,6-dihydroxy-benzoic acid 2-(2-methoxy-3,6-bis-methoxymethoxy-5-nitro-phenyl)-1-methyl-ethyl ester
CAS No.:884861-58-9
Molecular Formula:C₂₅H₃₀ClNO₁₁
Molecular Weight:555.966
Hs Code.:

Synonyms:2-but-3-enyl-3-chloro-4,6-dihydroxy-benzoic acid 2-(2-methoxy-3,6-bis-methoxymethoxy-5-nitro-phenyl)-1-methyl-ethyl ester

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Chemical Property of 2-but-3-enyl-3-chloro-4,6-dihydroxy-benzoic acid 2-(2-methoxy-3,6-bis-methoxymethoxy-5-nitro-phenyl)-1-methyl-ethyl ester

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Technology Process of 2-but-3-enyl-3-chloro-4,6-dihydroxy-benzoic acid 2-(2-methoxy-3,6-bis-methoxymethoxy-5-nitro-phenyl)-1-methyl-ethyl ester

There total 6 articles about 2-but-3-enyl-3-chloro-4,6-dihydroxy-benzoic acid 2-(2-methoxy-3,6-bis-methoxymethoxy-5-nitro-phenyl)-1-methyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 854261-03-3
1-(2-methoxy-3,6-bis(methoxymethoxy)-5-nitrophenyl)propan-2-ol

: 884861-57-8
2-but-3-enyl-3-chloro-4,6-dihydroxy-benzoic acid

: 884861-58-9
2-but-3-enyl-3-chloro-4,6-dihydroxy-benzoic acid 2-(2-methoxy-3,6-bis-methoxymethoxy-5-nitro-phenyl)-1-methyl-ethyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide;
DOI:10.1016/j.bmcl.2006.01.086 DOI:10.1021/jo061054f

Reference yield:

: 854261-02-2
1-(2-methoxy-3,6-bis(methoxymethoxy)phenyl)propan-2-ol

: 884861-58-9
2-but-3-enyl-3-chloro-4,6-dihydroxy-benzoic acid 2-(2-methoxy-3,6-bis-methoxymethoxy-5-nitro-phenyl)-1-methyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NH₄NO₃; (CF₃CO)2O / acetonitrile / 0.25 h / 20 °C

1.2: LiOH / tetrahydrofuran; methanol; H₂O / 0.08 h

2.1: 76 percent / DCC; DMAP

With ammonium nitrate; dmap; dicyclohexyl-carbodiimide; trifluoroacetic anhydride; In acetonitrile;
DOI:10.1021/jo061054f

Reference yield:

: 824-46-4
methoxyhydroquinone

: 884861-58-9
2-but-3-enyl-3-chloro-4,6-dihydroxy-benzoic acid 2-(2-methoxy-3,6-bis-methoxymethoxy-5-nitro-phenyl)-1-methyl-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 91 percent / NaH

2.1: n-BuLi

3.1: NH₄NO₃; (CF₃CO)2O / acetonitrile / 0.25 h / 20 °C

3.2: LiOH / tetrahydrofuran; methanol; H₂O / 0.08 h

4.1: 76 percent / DCC; DMAP

With ammonium nitrate; dmap; n-butyllithium; sodium hydride; dicyclohexyl-carbodiimide; trifluoroacetic anhydride; In acetonitrile;
DOI:10.1021/jo061054f