1-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(2R)-azido-3-tert-butyldiphenylsilyloxy propane

Base Information

Chemical Name:1-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(2R)-azido-3-tert-butyldiphenylsilyloxy propane
CAS No.:1403588-90-8
Molecular Formula:C₅₃H₅₉N₃O₆Si
Molecular Weight:862.153
Hs Code.:

Synonyms:1-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(2R)-azido-3-tert-butyldiphenylsilyloxy propane

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Chemical Property of 1-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(2R)-azido-3-tert-butyldiphenylsilyloxy propane

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Technology Process of 1-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(2R)-azido-3-tert-butyldiphenylsilyloxy propane

There total 3 articles about 1-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(2R)-azido-3-tert-butyldiphenylsilyloxy propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₄₂O₇

: 1403588-90-8
1-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(2R)-azido-3-tert-butyldiphenylsilyloxy propane

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 24 h / 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3: sodium azide / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere

With pyridine; sodium azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26078f

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1403588-90-8
1-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(2R)-azido-3-tert-butyldiphenylsilyloxy propane

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 24 h / 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3: sodium azide / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere

With pyridine; sodium azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26078f

Reference yield:

: 1403588-83-9
1-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(2S)-ol-3-tert-butyldiphenylsilyloxypropane

: 1403588-90-8
1-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(2R)-azido-3-tert-butyldiphenylsilyloxy propane

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere

With pyridine; sodium azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26078f