C₆₃H₆₄N₂S₅Si₂

Base Information

Chemical Name:C₆₃H₆₄N₂S₅Si₂
CAS No.:1352135-57-9
Molecular Formula:C₆₃H₆₄N₂S₅Si₂
Molecular Weight:1065.72
Hs Code.:

C<sub>63</sub>H<sub>64</sub>N<sub>2</sub>S<sub>5</sub>Si<sub>2</sub>

Synonyms:C₆₃H₆₄N₂S₅Si₂

Suppliers and Price of C₆₃H₆₄N₂S₅Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₃H₆₄N₂S₅Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₃H₆₄N₂S₅Si₂

There total 7 articles about C₆₃H₆₄N₂S₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1352135-55-7
C₅₃H₄₆Br₂N₂S₅

: 1066-54-2
trimethylsilylacetylene

: 1352135-57-9
C₆₃H₆₄N₂S₅Si₂

Guidance literature:: C₅₃H₄₆Br₂N₂S₅; With copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

trimethylsilylacetylene; In dichloromethane; at 0 ℃; Inert atmosphere; Reflux;
DOI:10.1016/j.jorganchem.2011.07.005

Reference yield:

: 1352135-53-5
C₄₅H₄₂Br₂N₂S₃

: 1352135-57-9
C₆₃H₆₄N₂S₅Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / Inert atmosphere; Reflux

2.1: N-Bromosuccinimide / tetrahydrofuran / 20 °C / Inert atmosphere; Darkness

3.1: copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere; Reflux

With N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene; 1.1: Stille cross-coupling / 3.1: Sonogashira coupling reaction / 3.2: Sonogashira coupling reaction;
DOI:10.1016/j.jorganchem.2011.07.005

Reference yield:

: 1352135-54-6
C₅₃H₄₈N₂S₅

: 1352135-57-9
C₆₃H₆₄N₂S₅Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / tetrahydrofuran / 20 °C / Inert atmosphere; Darkness

2.1: copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere; Reflux

With N-Bromosuccinimide; copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; 2.1: Sonogashira coupling reaction / 2.2: Sonogashira coupling reaction;
DOI:10.1016/j.jorganchem.2011.07.005