phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-β-D-glucopyranose

Base Information

Chemical Name:phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-β-D-glucopyranose
CAS No.:1401695-38-2
Molecular Formula:C₂₉H₄₃N₃O₅SSi
Molecular Weight:573.829
Hs Code.:

Synonyms:phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-β-D-glucopyranose

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Chemical Property of phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-β-D-glucopyranose

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Technology Process of phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-β-D-glucopyranose

There total 2 articles about phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: phenyl 2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-1-thio-D-glucopyranose

: 1401695-38-2
phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-β-D-glucopyranose

: 1401695-32-6
phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane

2: borane-THF; di-n-butylboryl trifluoromethanesulfonate

With borane-THF; di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ol202528k