[(1R,2S)-1-(3-Methoxy-phenyl)-2-phosphonooxy-propyl]-carbamic acid hexyl ester

Base Information

Chemical Name:[(1R,2S)-1-(3-Methoxy-phenyl)-2-phosphonooxy-propyl]-carbamic acid hexyl ester
CAS No.:526217-32-3
Molecular Formula:C₁₇H₂₈NO₇P
Molecular Weight:389.386
Hs Code.:

Synonyms:[(1R,2S)-1-(3-Methoxy-phenyl)-2-phosphonooxy-propyl]-carbamic acid hexyl ester

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Chemical Property of [(1R,2S)-1-(3-Methoxy-phenyl)-2-phosphonooxy-propyl]-carbamic acid hexyl ester

Chemical Property:

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Technology Process of [(1R,2S)-1-(3-Methoxy-phenyl)-2-phosphonooxy-propyl]-carbamic acid hexyl ester

There total 5 articles about [(1R,2S)-1-(3-Methoxy-phenyl)-2-phosphonooxy-propyl]-carbamic acid hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [(1R,2S)-2-(Bis-benzyloxy-phosphoryloxy)-1-(3-methoxy-phenyl)-propyl]-carbamic acid hexyl ester

: 526217-32-3
[(1R,2S)-1-(3-Methoxy-phenyl)-2-phosphonooxy-propyl]-carbamic acid hexyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 5.5h;
DOI:10.1016/S0968-0896(02)00380-2

Reference yield:

: 6092-54-2
n-hexyl chloroformate

: 526217-32-3
[(1R,2S)-1-(3-Methoxy-phenyl)-2-phosphonooxy-propyl]-carbamic acid hexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / NaHCO₃ / tetrahydrofuran; H₂O / 1 h / 0 - 20 °C

2: tetrazole / acetonitrile / 3 h / 20 °C

3: m-CPBA / CH₂Cl₂ / 1 h / 0 °C

4: H₂ / 10 percent Pd/C / methanol / 5.5 h / 20 °C

With 1H-tetrazole; hydrogen; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/S0968-0896(02)00380-2

Reference yield:

: 289051-64-5
hexyl (1R,2S)-2-hydroxy-1-(3-methoxyphenyl)propylcarbamate

: 526217-32-3
[(1R,2S)-1-(3-Methoxy-phenyl)-2-phosphonooxy-propyl]-carbamic acid hexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: tetrazole / acetonitrile / 3 h / 20 °C

2: m-CPBA / CH₂Cl₂ / 1 h / 0 °C

3: H₂ / 10 percent Pd/C / methanol / 5.5 h / 20 °C

With 1H-tetrazole; hydrogen; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0968-0896(02)00380-2