(1R,3R)-2-[2-(3-isopropyl-5,8-dioxo-5,8-dihydronaphthalen-1-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

Base Information

Chemical Name:(1R,3R)-2-[2-(3-isopropyl-5,8-dioxo-5,8-dihydronaphthalen-1-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid
CAS No.:1185024-72-9
Molecular Formula:C₂₆H₃₂O₄
Molecular Weight:408.538
Hs Code.:

Synonyms:(1R,3R)-2-[2-(3-isopropyl-5,8-dioxo-5,8-dihydronaphthalen-1-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,3R)-2-[2-(3-isopropyl-5,8-dioxo-5,8-dihydronaphthalen-1-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

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Technology Process of (1R,3R)-2-[2-(3-isopropyl-5,8-dioxo-5,8-dihydronaphthalen-1-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

There total 1 articles about (1R,3R)-2-[2-(3-isopropyl-5,8-dioxo-5,8-dihydronaphthalen-1-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 20-isopropyl-5,9-dimethyl-14,17-dioxopentacyco[10.6.2.0^1,10.0^4,9.0^13,18]icosa-13⁽¹⁸⁾,15,19-triene-5-caboxylic acid

: 1185024-72-9
(1R,3R)-2-[2-(3-isopropyl-5,8-dioxo-5,8-dihydronaphthalen-1-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

Guidance literature:: In 1,4-dioxane; at 130 ℃; for 10h;
DOI:10.1134/S1070428009010138

Reference yield: 55.0%

: 1185024-72-9
(1R,3R)-2-[2-(3-isopropyl-5,8-dioxo-5,8-dihydronaphthalen-1-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

: 59414-23-2
1-methoxy-3-<(trimethylsilyl)oxy>01,3-butadiene

: 1185024-75-2
(1R,3R)-2-[2-(7-hydroxy-3-isopropyl-9,10-dioxo-9,10-dihydroanthracen-1-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

Guidance literature:: With zinc(II) chloride; In tetrahydrofuran; at 20 ℃; for 30h; regioselective reaction; Inert atmosphere;
DOI:10.1134/S1070428009010138

Reference yield:

: 1185024-72-9
(1R,3R)-2-[2-(3-isopropyl-5,8-dioxo-5,8-dihydronaphthalen-1-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

: 4055-17-8
5-isopropenyl-2,3-dihydrothiophene 1,1-dioxide

: C₃₂H₃₆O₆S

: 2-[2-(8-isopropyl-4-methyl-3,3-dioxido-6,,11-dioxo-1,2,5,5a,6,11,11a,11b-octahydroanthra[2,1-b]thiophen-10-yl)ethyl]1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

: 2-[2-(8-isopropyl-4-methyl-3,3-dioxido-6,11-dioxo-1,2,5,5a,6,11,11a,11b-octahydroanthra[2,1-b]thiophen-10-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

: 2-[2-(9-isopropyl-4-methyl-3,3-dioxido-6,11-dioxo-1,2,5,5a,6,11,11a,11b-octahydroanthra[2,1-b]thiophen-7-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

: 2-[2-(9-isopropyl-4-methyl-3,3-dioxido-6,11-dioxo-1,2,5,5a,6,11,11a,11b-octahydroanthra[2,1-b]thiophen-7-yl)ethyl]-1,3-dimethyl-3-vinylcyclohexane-1-carboxylic acid

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 336h; Inert atmosphere;
DOI:10.1134/S1070428009010138