6-<methyl>amino>-2(R,S)-<<2-(trimethylsilyl)ethoxy>methoxy>-3(S)-<(phenylmethoxycarbonyl)amino>hexanoic acid

Base Information

• Chemical Name: 6-<methyl>amino>-2(R,S)-<<2-(trimethylsilyl)ethoxy>methoxy>-3(S)-<(phenylmethoxycarbonyl)amino>hexanoic acid
• CAS No.: 187155-13-1
• Molecular Formula: C₂₈H₄₂N₄O₈SSi
• Molecular Weight: 622.815

Synonyms:6-<methyl>amino>-2(R,S)-<<2-(trimethylsilyl)ethoxy>methoxy>-3(S)-<(phenylmethoxycarbonyl)amino>hexanoic acid

Chemical Property of 6-<methyl>amino>-2(R,S)-<<2-(trimethylsilyl)ethoxy>methoxy>-3(S)-<(phenylmethoxycarbonyl)amino>hexanoic acid

Chemical Property:

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Technology Process of 6-<methyl>amino>-2(R,S)-<<2-(trimethylsilyl)ethoxy>methoxy>-3(S)-<(phenylmethoxycarbonyl)amino>hexanoic acid

There total 1 articles about 6-<methyl>amino>-2(R,S)-<<2-(trimethylsilyl)ethoxy>methoxy>-3(S)-<(phenylmethoxycarbonyl)amino>hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C29H44N4O8SSi → 6-<methyl>amino>-2(R,S)-<<2-(trimethylsilyl)ethoxy>methoxy>-3(S)-<(phenylmethoxycarbonyl)amino>hexanoic acid (187155-13-1)

Guidance literature:

With lithium hydroxide; In 1,4-dioxane; water; for 4h; Yield given;

Reference yield: 90.0%

6-<methyl>amino>-2(R,S)-<<2-(trimethylsilyl)ethoxy>methoxy>-3(S)-<(phenylmethoxycarbonyl)amino>hexanoic acid (187155-13-1) + (S)-1-[(R)-2-(8-Amino-octanoylamino)-3-phenyl-propionyl]-pyrrolidine-2-carboxylic acid tert-butyl ester (187155-12-0) → C54H81N7O11SSi (187155-14-2)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide;

DOI:10.1016/S0960-894X(96)00554-9

Reference yield: 77.0%

D-phenylalanine tert-butyl ester (3081-28-5,6404-30-4,16367-71-8,16874-17-2) + 6-<methyl>amino>-2(R,S)-<<2-(trimethylsilyl)ethoxy>methoxy>-3(S)-<(phenylmethoxycarbonyl)amino>hexanoic acid (187155-13-1) → 2(R)-<<3(S)-<(benzyloxycarbonyl)amino>-6-<methyl>amino>-2(R,S)-<<2-(trimethylsilyl)ethoxy>methoxy>hexanoyl>amino>-3-phenylpropanoic acid tert-butyl ester

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In acetonitrile;

Downstream raw materials:

C₅₄H₈₁N₇O₁₁SSi

C₅₅H₈₃N₇O₁₁SSi

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