NSC₆₈₂₅₆₇

Base Information

• Chemical Name: NSC₆₈₂₅₆₇
• CAS No.: 127073-90-9
• Molecular Formula: C₁₈H₁₆O₅
• Molecular Weight: 312.322
• Mol file: 127073-90-9.mol

Synonyms:NSC₆₈₂₅₆₇

Chemical Property of NSC₆₈₂₅₆₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of NSC₆₈₂₅₆₇

There total 2 articles about NSC₆₈₂₅₆₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-Hydroxy-4-methoxybenzaldehyde (673-22-3) + homoveratric anhydride (55720-88-2) → NSC682567 (127073-90-9)

Guidance literature:

With potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride; In benzene; for 0.5h; Heating;

Reference yield:

2-Hydroxy-4-methoxybenzaldehyde (673-22-3) + (3,4-Dimethoxyphenyl)acetic acid (93-40-3) → NSC682567 (127073-90-9)

Guidance literature:

With potassium acetate; acetic anhydride; for 4h; Reflux;

DOI:10.1248/cpb.60.270

Reference yield: 67.0%

NSC682567 (127073-90-9) → (Z)-2-(2-(3,4-dimethoxyphenyl)-3-hydroxypropenyl)-5-methoxyphenol

Guidance literature:

With diisobutylaluminium hydride; In dichloromethane; cyclohexane; at -10 - 20 ℃; for 3.66667h; stereoselective reaction; Inert atmosphere;

DOI:10.1248/cpb.60.270

upstream raw materials:

2-Hydroxy-4-methoxybenzaldehyde

homoveratric anhydride

(3,4-Dimethoxyphenyl)acetic acid