<<3-<(6-chloropyridazin-3-yl)methyl>-4-methoxyphenyl>>-(2,4,6-trimethoxyphenyl)iodonium trifluoroacetate

Base Information

Chemical Name:<<3-<(6-chloropyridazin-3-yl)methyl>-4-methoxyphenyl>>-(2,4,6-trimethoxyphenyl)iodonium trifluoroacetate
CAS No.:116762-92-6
Molecular Formula:C₂F₃O₂*C₂₁H₂₁ClIN₂O₄
Molecular Weight:640.782
Hs Code.:

Synonyms:<<3-<(6-chloropyridazin-3-yl)methyl>-4-methoxyphenyl>>-(2,4,6-trimethoxyphenyl)iodonium trifluoroacetate

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Chemical Property of <<3-<(6-chloropyridazin-3-yl)methyl>-4-methoxyphenyl>>-(2,4,6-trimethoxyphenyl)iodonium trifluoroacetate

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Technology Process of <<3-<(6-chloropyridazin-3-yl)methyl>-4-methoxyphenyl>>-(2,4,6-trimethoxyphenyl)iodonium trifluoroacetate

There total 3 articles about <<3-<(6-chloropyridazin-3-yl)methyl>-4-methoxyphenyl>>-(2,4,6-trimethoxyphenyl)iodonium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116762-85-7
3-chloro-6-(5-iodo-2-methoxybenzyl)-pyridazine

: 116762-92-6
<<3-<(6-chloropyridazin-3-yl)methyl>-4-methoxyphenyl>>-(2,4,6-trimethoxyphenyl)iodonium trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / chlorine gas / CHCl₃

2: 1.) silver acetate, 3.) 40percentw/v sodium hydride / 1.) acetonitrile, 4 h, 2.) -30 deg C,1 h, 3.) CH₂Cl₂, RT, water

With silver(I) acetate; chlorine; sodium hydride; In chloroform;

Reference yield:

: 105190-14-5
bis<<3-<(6-chloropyridazin-3-yl)methyl>-4-methoxyphenyl>>iodonium trifluoroacetate

: 116762-92-6
<<3-<(6-chloropyridazin-3-yl)methyl>-4-methoxyphenyl>>-(2,4,6-trimethoxyphenyl)iodonium trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: copper bronze, triethylamine / CH₂Cl₂ / 18 h / Ambient temperature

2: 92 percent / chlorine gas / CHCl₃

3: 1.) silver acetate, 3.) 40percentw/v sodium hydride / 1.) acetonitrile, 4 h, 2.) -30 deg C,1 h, 3.) CH₂Cl₂, RT, water

With silver(I) acetate; chlorine; copper; sodium hydride; triethylamine; In dichloromethane; chloroform;

Reference yield:

: 621-23-8
1,2,3-trimethoxybenzene

: 120129-93-3
3-chloro-6-<5-(dichloroiodo)-2-methoxybenzyl>pyridazine

: 76-05-1
trifluoroacetic acid

: 116762-92-6
<<3-<(6-chloropyridazin-3-yl)methyl>-4-methoxyphenyl>>-(2,4,6-trimethoxyphenyl)iodonium trifluoroacetate

Guidance literature:: With silver(I) acetate; sodium hydride; Yield given. Multistep reaction; 1.) acetonitrile, 4 h, 2.) -30 deg C,1 h, 3.) CH₂Cl₂, RT, water;