2-bromo-N-(methoxymethyl)-N-aniline

Base Information

Chemical Name:2-bromo-N-(methoxymethyl)-N-aniline
CAS No.:81245-93-4
Molecular Formula:C₁₃H₁₄BrF₃N₂O₃
Molecular Weight:383.165
Hs Code.:

2-bromo-N-(methoxymethyl)-N-<N-methyl-N-(trifluoroacetyl)glycyl>aniline

Synonyms:2-bromo-N-(methoxymethyl)-N-aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-N-(methoxymethyl)-N-aniline

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Technology Process of 2-bromo-N-(methoxymethyl)-N-aniline

There total 3 articles about 2-bromo-N-(methoxymethyl)-N-aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35141-11-8
2-(2,2,2-trifluoro-N-methylacetamido)acetic acid

: 81245-93-4
2-bromo-N-(methoxymethyl)-N-aniline

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus pentachloride / diethyl ether / 3 h

2: 82 percent / benzene; ethyl acetate / 1 h / Ambient temperature

3: 1.) sodium hydride / 1.) THF, 0 deg C, 1.5 h, 2a.) 0 deg C, 30 min, 2b.) room temp., 3 h

With phosphorus pentachloride; sodium hydride; In diethyl ether; ethyl acetate; benzene;
DOI:10.1021/jo00133a042

Reference yield:

: 81245-91-2
N-(trifluoroacetyl)sarcosinyl chloride

: 81245-93-4
2-bromo-N-(methoxymethyl)-N-aniline

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / benzene; ethyl acetate / 1 h / Ambient temperature

2: 1.) sodium hydride / 1.) THF, 0 deg C, 1.5 h, 2a.) 0 deg C, 30 min, 2b.) room temp., 3 h

With sodium hydride; In ethyl acetate; benzene;
DOI:10.1021/jo00133a042

Reference yield:

: 81255-43-8
2-bromo-N-aniline

: 107-30-2
chloromethyl methyl ether

: 81245-93-4
2-bromo-N-(methoxymethyl)-N-aniline

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, 0 deg C, 1.5 h, 2a.) 0 deg C, 30 min, 2b.) room temp., 3 h;
DOI:10.1021/jo00133a042