1-methyl-3-(4-hydroxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione

Base Information

• Chemical Name: 1-methyl-3-(4-hydroxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione
• CAS No.: 158756-16-2
• Molecular Formula: C₁₂H₉F₃N₂O₃
• Molecular Weight: 286.21

Synonyms:1-methyl-3-(4-hydroxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione

Chemical Property of 1-methyl-3-(4-hydroxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione

Chemical Property:

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Technology Process of 1-methyl-3-(4-hydroxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione

There total 1 articles about 1-methyl-3-(4-hydroxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-3-(4-methoxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione (158756-15-1) → 1-methyl-3-(4-hydroxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione (158756-16-2)

Guidance literature:

With boron tribromide; In dichloromethane;

Reference yield:

1-methyl-3-(4-hydroxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione (158756-16-2) + 1-Chloro-4-(chloromethyl)benzene (104-83-6) → 3-[4-(4-chlorophenylmethoxy)phenyl]-1-methyl-6-trifluoromethyluracil

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

methyl 2-(2-(chloromethyl)-5-methylphenoxy)propanoate (154079-77-3) + 1-methyl-3-(4-hydroxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione (158756-16-2) + Methyl 2-?2-[4-(4-difluoromethyl-4,5-dihydro-3-methyl-1,2,4-triazol-5(1H)-on-1-yl)-3-fluorophenoxymethyl]-5-methylphen[oxy]propionate → methyl 2-[2-[4-(1-methyl-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedion-3-yl)phenoxymethyl]-5-methylphenoxy]propionate (158755-92-1) + METHYL 2-[2[4-1-METHYL-7-TRIFLUOROMETHYL-2,4-(1H,3H)-PYRIMIDINEDION-3-YL)PHENOXYMETHYL]-5-METHYLPHENOXY]PROPIONATE

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide;

upstream raw materials:

1-methyl-3-(4-methoxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione

Downstream raw materials:

methyl 2-[2-[4-(1-methyl-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedion-3-yl)phenoxymethyl]-5-methylphenoxy]propionate

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