nonanoic acid 2-ethynyl-5-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide

Base Information

Chemical Name:nonanoic acid 2-ethynyl-5-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide
CAS No.:859172-18-2
Molecular Formula:C₂₃H₃₅NO₅
Molecular Weight:405.535
Hs Code.:

Synonyms:nonanoic acid 2-ethynyl-5-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of nonanoic acid 2-ethynyl-5-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide

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Technology Process of nonanoic acid 2-ethynyl-5-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide

There total 4 articles about nonanoic acid 2-ethynyl-5-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 875153-08-5
nonanoic acid 5-methoxy-4-(2-methoxy-ethoxymethoxy)-2-trimethylsilanylethynyl-benzylamide

: 859172-18-2
nonanoic acid 2-ethynyl-5-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 2.5h;
DOI:10.1021/jm050139q

Reference yield:

: nonanoic acid 3-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide

: 859172-18-2
nonanoic acid 2-ethynyl-5-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: CF₃COOAg; iodine / CHCl₃ / 20 °C

2: pyrrolidine; (Ph₃)4Pd; CuI / benzene / 20 °C

3: 1.23 g / KOH / methanol / 2.5 h / 20 °C

With pyrrolidine; potassium hydroxide; copper(l) iodide; (Ph₃)4Pd; iodine; silver trifluoroacetate; In methanol; chloroform; benzene; 2: Sonogashira coupling;
DOI:10.1021/jm050139q

Reference yield:

: nonanoic acid 2-iodo-5-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide

: 859172-18-2
nonanoic acid 2-ethynyl-5-methoxy-4-(2-methoxy-ethoxymethoxy)-benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyrrolidine; (Ph₃)4Pd; CuI / benzene / 20 °C

2: 1.23 g / KOH / methanol / 2.5 h / 20 °C

With pyrrolidine; potassium hydroxide; copper(l) iodide; (Ph₃)4Pd; In methanol; benzene; 1: Sonogashira coupling;
DOI:10.1021/jm050139q