Selenophosphoric acid Se-(3-methyl-2-oxo-1-phenyl-butyl) ester O,O'-diphenyl ester

Base Information

• Chemical Name: Selenophosphoric acid Se-(3-methyl-2-oxo-1-phenyl-butyl) ester O,O'-diphenyl ester
• CAS No.: 137224-95-4
• Molecular Formula: C₂₃H₂₃O₄PSe
• Molecular Weight: 473.367

Synonyms:Selenophosphoric acid Se-(3-methyl-2-oxo-1-phenyl-butyl) ester O,O'-diphenyl ester

Chemical Property of Selenophosphoric acid Se-(3-methyl-2-oxo-1-phenyl-butyl) ester O,O'-diphenyl ester

Chemical Property:

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Technology Process of Selenophosphoric acid Se-(3-methyl-2-oxo-1-phenyl-butyl) ester O,O'-diphenyl ester

There total 1 articles about Selenophosphoric acid Se-(3-methyl-2-oxo-1-phenyl-butyl) ester O,O'-diphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methyl-1-phenylbutan-2-one (2893-05-2) + C18H15ClO3PSe(1+)*ClO2S(1-) → Selenophosphoric acid Se-(3-methyl-2-oxo-1-phenyl-butyl) ester O,O'-diphenyl ester (137224-95-4)

Guidance literature:

In dichloromethane; at -20 ℃;

DOI:10.1016/S0040-4039(00)92177-4

Reference yield: 64.0%

Selenophosphoric acid Se-(3-methyl-2-oxo-1-phenyl-butyl) ester O,O'-diphenyl ester (137224-95-4) → (Z)-3-methyl-1-phenylbut-1-ene (15325-56-1)

Guidance literature:

With sodium tetrahydroborate; In methanol; Heating;

DOI:10.1016/S0040-4039(00)92177-4

Reference yield:

Selenophosphoric acid Se-(3-methyl-2-oxo-1-phenyl-butyl) ester O,O'-diphenyl ester (137224-95-4) → (2S,3R)-2-Isopropyl-3-phenyl-selenirane

Guidance literature:

With sodium tetrahydroborate; In methanol; Ambient temperature;

DOI:10.1016/S0040-4039(00)92177-4

upstream raw materials:

3-methyl-1-phenylbutan-2-one

Downstream raw materials:

(Z)-3-methyl-1-phenylbut-1-ene

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