10,13,16-tris(p-tolylsulfonyl)-10,13,16-triazapentaicosane-1,25-diyl bis(methanesulfonate)

Base Information

Chemical Name:10,13,16-tris(p-tolylsulfonyl)-10,13,16-triazapentaicosane-1,25-diyl bis(methanesulfonate)
CAS No.:106961-27-7
Molecular Formula:C₄₅H₇₁N₃O₁₂S₅
Molecular Weight:1006.4
Hs Code.:

Synonyms:10,13,16-tris(p-tolylsulfonyl)-10,13,16-triazapentaicosane-1,25-diyl bis(methanesulfonate)

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Chemical Property of 10,13,16-tris(p-tolylsulfonyl)-10,13,16-triazapentaicosane-1,25-diyl bis(methanesulfonate)

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Technology Process of 10,13,16-tris(p-tolylsulfonyl)-10,13,16-triazapentaicosane-1,25-diyl bis(methanesulfonate)

There total 5 articles about 10,13,16-tris(p-tolylsulfonyl)-10,13,16-triazapentaicosane-1,25-diyl bis(methanesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3937-56-2
1,9-Nonanediol

: 106961-27-7
10,13,16-tris(p-tolylsulfonyl)-10,13,16-triazapentaicosane-1,25-diyl bis(methanesulfonate)

Guidance literature:: Multi-step reaction with 5 steps

1: conc. HCl / tetrahydrofuran / 7 h / Ambient temperature

2: 98 percent / Et₃N / CH₂Cl₂ / 1.) -18 deg C, 20 min, 2.) RT, 2 h

3: 72 percent / dimethylformamide / 6 h / 95 °C

4: 70 percent / TsOH / ethanol; H₂O / 1.) reflux, 8 h, 2.) RT, 12 h

5: Et₃N / CH₂Cl₂ / -18 deg C, RT, 18 h

With toluene-4-sulfonic acid; triethylamine; hydrogenchloride; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19860690308

Reference yield:

: 98847-00-8
9-<(2H-tetrahydropyran-2-yl)oxy>nonan-1-ol

: 106961-27-7
10,13,16-tris(p-tolylsulfonyl)-10,13,16-triazapentaicosane-1,25-diyl bis(methanesulfonate)

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / Et₃N / CH₂Cl₂ / 1.) -18 deg C, 20 min, 2.) RT, 2 h

2: 72 percent / dimethylformamide / 6 h / 95 °C

3: 70 percent / TsOH / ethanol; H₂O / 1.) reflux, 8 h, 2.) RT, 12 h

4: Et₃N / CH₂Cl₂ / -18 deg C, RT, 18 h

With toluene-4-sulfonic acid; triethylamine; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19860690308

Reference yield:

: 106961-25-5
10,13,16-tris(p-tolylsulfonyl)-1,25-bis<(2H-tetrahydropyran-2-yl)oxy>-10,13,16-triazapentaicosane

: 106961-27-7
10,13,16-tris(p-tolylsulfonyl)-10,13,16-triazapentaicosane-1,25-diyl bis(methanesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / TsOH / ethanol; H₂O / 1.) reflux, 8 h, 2.) RT, 12 h

2: Et₃N / CH₂Cl₂ / -18 deg C, RT, 18 h

With toluene-4-sulfonic acid; triethylamine; In ethanol; dichloromethane; water;
DOI:10.1002/hlca.19860690308