((R)-1-(benzyloxy)-9-((2S,5S)-5-((S)-oxiran-2-yl)-tetrahydrofuran-2-yl)nonan-2-yloxy)(tert-butyl)dimethylsilane

Base Information

• Chemical Name: ((R)-1-(benzyloxy)-9-((2S,5S)-5-((S)-oxiran-2-yl)-tetrahydrofuran-2-yl)nonan-2-yloxy)(tert-butyl)dimethylsilane
• CAS No.: 1033883-69-0
• Molecular Formula: C₂₈H₄₈O₄Si
• Molecular Weight: 476.772

Synonyms:((R)-1-(benzyloxy)-9-((2S,5S)-5-((S)-oxiran-2-yl)-tetrahydrofuran-2-yl)nonan-2-yloxy)(tert-butyl)dimethylsilane

Chemical Property of ((R)-1-(benzyloxy)-9-((2S,5S)-5-((S)-oxiran-2-yl)-tetrahydrofuran-2-yl)nonan-2-yloxy)(tert-butyl)dimethylsilane

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Technology Process of ((R)-1-(benzyloxy)-9-((2S,5S)-5-((S)-oxiran-2-yl)-tetrahydrofuran-2-yl)nonan-2-yloxy)(tert-butyl)dimethylsilane

There total 1 articles about ((R)-1-(benzyloxy)-9-((2S,5S)-5-((S)-oxiran-2-yl)-tetrahydrofuran-2-yl)nonan-2-yloxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C32H50N2O5SSi (1033883-55-4) → ((R)-1-(benzyloxy)-9-((2S,5S)-5-((S)-oxiran-2-yl)-tetrahydrofuran-2-yl)nonan-2-yloxy)(tert-butyl)dimethylsilane (1033883-69-0)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In toluene; at 80 ℃; for 0.416667h; Inert atmosphere;

DOI:10.1021/ol800767e

Reference yield: 98.0%

((R)-1-(benzyloxy)-9-((2S,5S)-5-((S)-oxiran-2-yl)-tetrahydrofuran-2-yl)nonan-2-yloxy)(tert-butyl)dimethylsilane (1033883-69-0) + trimethylsulphonium iodide (2181-42-2) → (S)-1-((2S,5S)-5-((R)-9-(benzyloxy)-8-(tert-butyldimethylsilyloxy)nonyl)-tetrahydrofuran-2-yl)prop-2-en-1-ol (1033883-45-2)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at -10 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol800767e

upstream raw materials:

C₃₂H₅₀N₂O₅SSi

Downstream raw materials:

(S)-1-((2S,5S)-5-((R)-9-(benzyloxy)-8-(tert-butyldimethylsilyloxy)nonyl)-tetrahydrofuran-2-yl)prop-2-en-1-ol

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