2-(1-(4-bromophenethyl)piperidin-4-yl)-1-(2-ethoxyethyl)-1H-benzo[d]imidazole

Base Information

Chemical Name:2-(1-(4-bromophenethyl)piperidin-4-yl)-1-(2-ethoxyethyl)-1H-benzo[d]imidazole
CAS No.:1567835-74-8
Molecular Formula:C₂₄H₃₀BrN₃O
Molecular Weight:456.426
Hs Code.:

Synonyms:2-(1-(4-bromophenethyl)piperidin-4-yl)-1-(2-ethoxyethyl)-1H-benzo[d]imidazole

Suppliers and Price of 2-(1-(4-bromophenethyl)piperidin-4-yl)-1-(2-ethoxyethyl)-1H-benzo[d]imidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-(1-(4-bromophenethyl)piperidin-4-yl)-1-(2-ethoxyethyl)-1H-benzo[d]imidazole

Chemical Property:

Purity/Quality:: 95%-98% ^*data from raw suppliers

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Technology Process of 2-(1-(4-bromophenethyl)piperidin-4-yl)-1-(2-ethoxyethyl)-1H-benzo[d]imidazole

There total 9 articles about 2-(1-(4-bromophenethyl)piperidin-4-yl)-1-(2-ethoxyethyl)-1H-benzo[d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1567835-76-0
1-(4-bromophenethyl)-N-(2-((2-ethoxyethyl)amino)phenyl)piperidine-4-carboxamide

: 1567835-74-8
2-(1-(4-bromophenethyl)piperidin-4-yl)-1-(2-ethoxyethyl)-1H-benzo[d]imidazole

Guidance literature:: With acetic acid; at 125 ℃; for 18h; Inert atmosphere;

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1567835-74-8
2-(1-(4-bromophenethyl)piperidin-4-yl)-1-(2-ethoxyethyl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / 2-methyltetrahydrofuran; dimethyl sulfoxide / 23.5 h / 10 - 45 °C / Inert atmosphere

2: 5%-palladium/activated carbon; hydrogen / ethanol / 3 h / 5 - 10 °C / 2250.23 - 3000.3 Torr

3: potassium tert-butylate / N,N-dimethyl-formamide; toluene / 29 h / -2 - 100 °C / Inert atmosphere; Cooling

With 5%-palladium/activated carbon; potassium tert-butylate; hydrogen; potassium carbonate; In 2-methyltetrahydrofuran; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 95893-88-2
N-(β-ethoxyethyl)-o-nitroaniline

: 1567835-74-8
2-(1-(4-bromophenethyl)piperidin-4-yl)-1-(2-ethoxyethyl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 5%-palladium/activated carbon; hydrogen / ethanol / 3 h / 5 - 10 °C / 2250.23 - 3000.3 Torr

2: potassium tert-butylate / N,N-dimethyl-formamide; toluene / 29 h / -2 - 100 °C / Inert atmosphere; Cooling

With 5%-palladium/activated carbon; potassium tert-butylate; hydrogen; In ethanol; N,N-dimethyl-formamide; toluene;