5-bromo-β,β,2,4-tetramethyl-3,6-dioxo-1,4-cyclohexadiene-1-propanoic acid

Base Information

Chemical Name:5-bromo-β,β,2,4-tetramethyl-3,6-dioxo-1,4-cyclohexadiene-1-propanoic acid
CAS No.:121031-01-4
Molecular Formula:C₁₃H₁₅BrO₄
Molecular Weight:315.164
Hs Code.:

Synonyms:5-bromo-β,β,2,4-tetramethyl-3,6-dioxo-1,4-cyclohexadiene-1-propanoic acid

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Chemical Property of 5-bromo-β,β,2,4-tetramethyl-3,6-dioxo-1,4-cyclohexadiene-1-propanoic acid

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Technology Process of 5-bromo-β,β,2,4-tetramethyl-3,6-dioxo-1,4-cyclohexadiene-1-propanoic acid

There total 8 articles about 5-bromo-β,β,2,4-tetramethyl-3,6-dioxo-1,4-cyclohexadiene-1-propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 8-bromo-6-hydroxy-4,4,5,7-tetramethyl-chroman-2-one

: 121031-01-4
5-bromo-β,β,2,4-tetramethyl-3,6-dioxo-1,4-cyclohexadiene-1-propanoic acid

Guidance literature:: With N-Bromosuccinimide; In water; acetonitrile;

Reference yield: 80.0%

: 50442-68-7
6-hydroxy-4,4,5,7-tetramethyl-3,4-dihydrocoumarin

: 121031-01-4
5-bromo-β,β,2,4-tetramethyl-3,6-dioxo-1,4-cyclohexadiene-1-propanoic acid

Guidance literature:: With bromine; acetic acid; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/acsmedchemlett.5b00146

Reference yield:

: 541-47-9
3-Methylbutenoic acid

: 121031-01-4
5-bromo-β,β,2,4-tetramethyl-3,6-dioxo-1,4-cyclohexadiene-1-propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: MeSO₃H / 70 °C

2: 100 percent / N-bromosuccinimide / acetonitrile; H₂O / 20 °C

With N-Bromosuccinimide; methanesulfonic acid; In water; acetonitrile;