5-amino-1-(1-benzhydryl-azetidin-3-yl)-1H-pyrazole-4-carboxylic acid amide

Base Information

Chemical Name:5-amino-1-(1-benzhydryl-azetidin-3-yl)-1H-pyrazole-4-carboxylic acid amide
CAS No.:1025713-59-0
Molecular Formula:C₂₀H₂₁N₅O
Molecular Weight:347.42
Hs Code.:

Synonyms:5-amino-1-(1-benzhydryl-azetidin-3-yl)-1H-pyrazole-4-carboxylic acid amide

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Chemical Property of 5-amino-1-(1-benzhydryl-azetidin-3-yl)-1H-pyrazole-4-carboxylic acid amide

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Technology Process of 5-amino-1-(1-benzhydryl-azetidin-3-yl)-1H-pyrazole-4-carboxylic acid amide

There total 6 articles about 5-amino-1-(1-benzhydryl-azetidin-3-yl)-1H-pyrazole-4-carboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1025713-69-2
C₂₀H₁₉N₅

: 1025713-59-0
5-amino-1-(1-benzhydryl-azetidin-3-yl)-1H-pyrazole-4-carboxylic acid amide

Guidance literature:: C₂₀H₁₉N₅; With sulfuric acid; at 0 - 45 ℃; for 3h;

With ammonia; water;

Reference yield:

: 18621-17-5
1-(diphenylmethyl)-3-hydroxyazetidine

: 1025713-59-0
5-amino-1-(1-benzhydryl-azetidin-3-yl)-1H-pyrazole-4-carboxylic acid amide

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine-SO₃ complex; triethylamine / tetrahydrofuran; dimethyl sulfoxide / 2.17 h

2.1: acetic acid / methanol / 18 h

3.1: sodium cyanoborohydride; acetic acid / 5 h

3.2: pH 7

4.1: hydrogenchloride / 1,4-dioxane / 3 h

5.1: triethylamine / ethanol / 16 h / 90 °C

6.1: sulfuric acid / 3 h / 0 - 45 °C

With hydrogenchloride; pyridine-SO₃ complex; sulfuric acid; sodium cyanoborohydride; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dimethyl sulfoxide;

Reference yield:

: (1-benzhydryl-azetidin-3-yl)-hydrazine trihydrochloride

: 1025713-59-0
5-amino-1-(1-benzhydryl-azetidin-3-yl)-1H-pyrazole-4-carboxylic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / 16 h / 90 °C

2: sulfuric acid / 3 h / 0 - 45 °C

With sulfuric acid; triethylamine; In ethanol;