Technology Process of C53H82N6O9SSi
There total 20 articles about C53H82N6O9SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine;
In
N,N-dimethyl-formamide;
for 4h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dmap / dichloromethane / 4 h / 20 °C
2: tetrahydrofuran / 16 h / 60 °C
3: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C
4: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h
With
hydrogenchloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine;
dmap;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / dichloromethane / 2 h / 20 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
3: triethylamine / dmap / dichloromethane / 4 h / 20 °C
4: tetrahydrofuran / 16 h / 60 °C
5: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C
6: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h
With
hydrogenchloride; tetrabutyl ammonium fluoride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine;
dmap;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;