C₄₆H₆₆N₆O₆

Base Information

• Chemical Name: C₄₆H₆₆N₆O₆
• CAS No.: 1009094-32-9
• Molecular Formula: C₄₆H₆₆N₆O₆
• Molecular Weight: 799.067
• Mol file: 1009094-32-9.mol

Synonyms:C₄₆H₆₆N₆O₆

Chemical Property of C₄₆H₆₆N₆O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₆H₆₆N₆O₆

There total 12 articles about C₄₆H₆₆N₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

C46H64N8O6 (1009094-35-2) → C46H66N6O6 (1009094-32-9)

Guidance literature:

With 1,4-dithio-L-threitol; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

Reference yield:

C12H14BrNO4 (1009091-84-2) → C46H66N6O6 (1009094-32-9)

Guidance literature:

Multi-step reaction with 7 steps

1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

1.2: 1 h

2.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C

3.2: 2 h

3.3: 5 h

4.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.17 h

4.2: 1 h / 70 °C

5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 0.17 h / 20 °C

5.2: 2 h / 20 °C

6.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 1 h / 20 °C

7.1: 1,4-dithio-L-threitol; 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.33 h / 0 °C

With titanium(IV) isopropylate; 1,4-dithio-L-threitol; potassium acetate; diisobutylaluminium hydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; pyridine; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

C9H10BrNO2 → C46H66N6O6 (1009094-32-9)

Guidance literature:

Multi-step reaction with 9 steps

1.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2

1.2: pH 7 / Alkaline aqueous solution

2.1: benzene / Heating / reflux

3.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

3.2: 1 h

4.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C

5.2: 2 h

5.3: 5 h

6.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.17 h

6.2: 1 h / 70 °C

7.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 0.17 h / 20 °C

7.2: 2 h / 20 °C

8.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 1 h / 20 °C

9.1: 1,4-dithio-L-threitol; 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.33 h / 0 °C

With titanium(IV) isopropylate; hydrogenchloride; 1,4-dithio-L-threitol; methyl orange; potassium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; benzene;

upstream raw materials:

C₄₆H₆₄N₈O₆

C₈H₁₀BNO₄

C₁₂H₁₄BrNO₄

C₁₆H₂₀BrNO₅