methyl (E)-3-<2-(4-acetoxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate

Base Information

• Chemical Name: methyl (E)-3-<2-(4-acetoxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate
• CAS No.: 162662-81-9
• Molecular Formula: C₂₄H₂₂O₉
• Molecular Weight: 454.433
• Mol file: 162662-81-9.mol

Synonyms:methyl (E)-3-<2-(4-acetoxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate

Chemical Property of methyl (E)-3-<2-(4-acetoxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl (E)-3-<2-(4-acetoxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate

There total 1 articles about methyl (E)-3-<2-(4-acetoxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl (E)-3-<(2R*,3R*)-2,3-dihydro-2-(4-acetoxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate → methyl (E)-3-<2-(4-acetoxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate (162662-81-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; for 40h; Heating;

DOI:10.1248/cpb.42.2536

Reference yield: 85.0%

methyl (E)-3-<2-(4-acetoxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate (162662-81-9) → methyl (E)-3-<2-(4-hydroxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate

Guidance literature:

With sodium methylate; In methanol; dichloromethane; at 0 ℃; for 1h;

DOI:10.1248/cpb.42.2536

Reference yield: 81.0%

methyl (E)-3-<2-(4-acetoxy-2-methoxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate (162662-81-9) → methyl (E)-3-<2-(4-acetoxy-2-hydroxyphenyl)-6-methoxy-3-methoxycarbonylbenzofuran-5-yl>propenoate

Guidance literature:

With boron tribromide; In dichloromethane; at -78 ℃; for 4h;

DOI:10.1248/cpb.42.2536