Methyl 2,3-dideoxy-4,6-O-isopropylidene-2,3-(N-tosylepimino)-α-D-allopyranoside

Base Information

Chemical Name:Methyl 2,3-dideoxy-4,6-O-isopropylidene-2,3-(N-tosylepimino)-α-D-allopyranoside
CAS No.:143366-47-6
Molecular Formula:C₁₇H₂₃NO₆S
Molecular Weight:369.439
Hs Code.:

Synonyms:Methyl 2,3-dideoxy-4,6-O-isopropylidene-2,3-(N-tosylepimino)-α-D-allopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2,3-dideoxy-4,6-O-isopropylidene-2,3-(N-tosylepimino)-α-D-allopyranoside

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Technology Process of Methyl 2,3-dideoxy-4,6-O-isopropylidene-2,3-(N-tosylepimino)-α-D-allopyranoside

There total 5 articles about Methyl 2,3-dideoxy-4,6-O-isopropylidene-2,3-(N-tosylepimino)-α-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 143366-46-5
Methyl 2-deoxy-4,6-O-isopropylidene-3-O-tosyl-2-tosylamido-α-D-glucopyranoside

: 143366-47-6
Methyl 2,3-dideoxy-4,6-O-isopropylidene-2,3-(N-tosylepimino)-α-D-allopyranoside

Guidance literature:: With sodium hydroxide; In methanol; at 40 ℃; for 6h;
DOI:10.1016/S0008-6215(00)90515-9

Reference yield: 3.0%

: 143366-51-2
Methyl 2,3-dideoxy-2-fluoro-4,6-O-isopropylidene-3-tosylamido-α-D-altropyranoside

: 143366-47-6
Methyl 2,3-dideoxy-4,6-O-isopropylidene-2,3-(N-tosylepimino)-α-D-allopyranoside

: 143366-52-3
Methyl 2,3-dideoxy-3-fluoro-4,6-O-isopropylidene-2-tosylamido-α-D-glucopyranoside

Guidance literature:: With potassium hydrogen bifluoride; In N,N-dimethyl-formamide; at 150 ℃; for 6h;
DOI:10.1016/S0008-6215(00)90515-9

Reference yield:

: 56838-15-4
((4aR,6S,7R,8R,8aS)-8-Hydroxy-6-methoxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-carbamic acid methyl ester

: 143366-47-6
Methyl 2,3-dideoxy-4,6-O-isopropylidene-2,3-(N-tosylepimino)-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / aq. 2 M NaOH / dioxane / 2 h / Heating

2: 84 percent / Na₂CO₃ / dioxane; H₂O / 2 h / 0 °C

3: 78 percent / pyridine / 26 h / 90 °C

4: 81 percent / 0.5 M NaOH / methanol / 6 h / 40 °C

With pyridine; sodium hydroxide; sodium carbonate; In 1,4-dioxane; methanol; water;
DOI:10.1016/S0008-6215(00)90515-9