Technology Process of C41H58O10
There total 29 articles about C41H58O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
hexane; dichloromethane;
at -80 - -40 ℃;
for 1.58333h;
DOI:10.1016/S0040-4020(02)00660-9
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
dichloromethane;
at -80 - -30 ℃;
for 2h;
DOI:10.1039/b009506k
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99 percent / hydrogen; AcOH / Pd(OH)2/C / ethyl acetate; methanol / 72 h / 20 °C
2: 174 mg / 10-camphorsulfonic acid / tetrahydrofuran / 1 h / 20 °C
3: 100 percent / N,N-diisopropylethylamine / 1,2-dichloro-ethane / 14 h / 40 °C
4: 100 percent / diisobutylaluminum hydride / CH2Cl2; hexane / 1.58 h / -80 - -40 °C
With
(1S)-10-camphorsulfonic acid; hydrogen; diisobutylaluminium hydride; acetic acid; N-ethyl-N,N-diisopropylamine;
palladium dihydroxide;
In
tetrahydrofuran; methanol; hexane; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4020(02)00660-9