4-hydroxy-1,2-diphenyl-1-[4-[2-N,N-dimethylamino]ethoxy]-phenyl-1-butene

Base Information

• Chemical Name: 4-hydroxy-1,2-diphenyl-1-[4-[2-N,N-dimethylamino]ethoxy]-phenyl-1-butene
• CAS No.: 1262682-37-0
• Molecular Formula: C₂₆H₂₉NO₂
• Molecular Weight: 387.522

Synonyms:4-hydroxy-1,2-diphenyl-1-[4-[2-N,N-dimethylamino]ethoxy]-phenyl-1-butene

Chemical Property of 4-hydroxy-1,2-diphenyl-1-[4-[2-N,N-dimethylamino]ethoxy]-phenyl-1-butene

Chemical Property:

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Technology Process of 4-hydroxy-1,2-diphenyl-1-[4-[2-N,N-dimethylamino]ethoxy]-phenyl-1-butene

There total 1 articles about 4-hydroxy-1,2-diphenyl-1-[4-[2-N,N-dimethylamino]ethoxy]-phenyl-1-butene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-acetoxy-1,2-diphenyl-1-[4-[2-(N,N-dimethylamino) ethoxy]-phenyl]-1-butene → 4-hydroxy-1,2-diphenyl-1-[4-[2-N,N-dimethylamino]ethoxy]-phenyl-1-butene (1262682-37-0)

Guidance literature:

4-acetoxy-1,2-diphenyl-1-[4-[2-(N,N-dimethylamino) ethoxy]-phenyl]-1-butene; With water; sodium hydroxide; In methanol; at 70 - 72 ℃; for 4h;

With hydrogenchloride; In methanol; water; at 20 ℃; pH=8 - 8.5;

Reference yield:

4-hydroxy-1,2-diphenyl-1-[4-[2-N,N-dimethylamino]ethoxy]-phenyl-1-butene (1262682-37-0) → toremifene (89778-26-7)

Guidance literature:

4-hydroxy-1,2-diphenyl-1-[4-[2-N,N-dimethylamino]ethoxy]-phenyl-1-butene; With thionyl chloride; In dichloromethane; at 20 - 42 ℃; for 7h;

With ammonia; In water; ethyl acetate; pH=8.1 - 8.3;

Downstream raw materials:

toremifene

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