6,8-dihydroxy-7-o-tolylquinoline

Base Information

Chemical Name:6,8-dihydroxy-7-o-tolylquinoline
CAS No.:1300014-94-1
Molecular Formula:C₁₆H₁₃NO₂
Molecular Weight:251.285
Hs Code.:

Synonyms:6,8-dihydroxy-7-o-tolylquinoline

Suppliers and Price of 6,8-dihydroxy-7-o-tolylquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6,8-dihydroxy-7-o-tolylquinoline

Chemical Property:

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Technology Process of 6,8-dihydroxy-7-o-tolylquinoline

There total 4 articles about 6,8-dihydroxy-7-o-tolylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300015-01-3
6,8-dimethoxy-7-o-tolylquinoline

: 1300014-94-1
6,8-dihydroxy-7-o-tolylquinoline

Guidance literature:: 6,8-dimethoxy-7-o-tolylquinoline; With boron tribromide; In dichloromethane; at -78 - 20 ℃;

With water; sodium hydrogencarbonate; In dichloromethane; Cooling with ice;

Reference yield:

: 1300014-98-5
2,6-dimethoxy-2'-methyl-3-nitrobiphenyl

: 1300014-94-1
6,8-dihydroxy-7-o-tolylquinoline

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium on carbon / methanol / 2 h / 50 °C / 760.05 Torr

2.1: hydrogenchloride / water / 2 h / 90 °C

3.1: boron tribromide / dichloromethane / -78 - 20 °C

3.2: Cooling with ice

With hydrogenchloride; hydrogen; boron tribromide; palladium on carbon; In methanol; dichloromethane; water;

Reference yield:

: 1300014-97-4
2-iodo-1,3-dimethoxy-4-nitrobenzene

: 1300014-94-1
6,8-dihydroxy-7-o-tolylquinoline

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; acetonitrile; water / 32 h / 90 °C

2.1: hydrogen / palladium on carbon / methanol / 2 h / 50 °C / 760.05 Torr

3.1: hydrogenchloride / water / 2 h / 90 °C

4.1: boron tribromide / dichloromethane / -78 - 20 °C

4.2: Cooling with ice

With hydrogenchloride; hydrogen; boron tribromide; potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium on carbon; In 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;