3-methyl-1-(4-methylphenyl)-1,2-diaza-3-azoniacyclopent-3-en-5-one

Base Information

Chemical Name:3-methyl-1-(4-methylphenyl)-1,2-diaza-3-azoniacyclopent-3-en-5-one
CAS No.:5176-32-9
Molecular Formula:C₁₅H₁₉NO₂
Molecular Weight:245.321
Hs Code.:
Mol file:5176-32-9.mol

Synonyms:Naphthalen-1,4-imine-9-carboxylicacid, 1,2,3,4-tetrahydro-, tert-butyl ester (7CI,8CI)

Suppliers and Price of 3-methyl-1-(4-methylphenyl)-1,2-diaza-3-azoniacyclopent-3-en-5-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 11 raw suppliers

Chemical Property of 3-methyl-1-(4-methylphenyl)-1,2-diaza-3-azoniacyclopent-3-en-5-one

Chemical Property:

Melting Point:41-42℃
Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：29.54000
Density:g/cm³
LogP:3.75120

Purity/Quality:: 99.0% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-methyl-1-(4-methylphenyl)-1,2-diaza-3-azoniacyclopent-3-en-5-one

There total 8 articles about 3-methyl-1-(4-methylphenyl)-1,2-diaza-3-azoniacyclopent-3-en-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 5176-28-3
N-(tert-butoxycarbonyl)-1,4-dihydro-1,4-iminonaphthalene

: 5176-32-9
tert-butyl 1,2,3,4-tetrahydro-1,4-epiminonaphthalene-9-carboxylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 1.5h;
DOI:10.1021/ja036644z

Reference yield: 90.0%

: N-(tert-butoxycarbonyl)-exo-2-(methylsulfanylthiocarbonyloxy)-1,2,3,4-tetrahydro-1,4-iminonaphthalene

: 5176-32-9
tert-butyl 1,2,3,4-tetrahydro-1,4-epiminonaphthalene-9-carboxylate

: 484698-23-9
N-(tert-butoxycarbonyl)-1,2,3,4-tetrahydro-1,4-methanoisoquinoline

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In toluene; for 2.16667h; Heating;
DOI:10.1021/ol027039o

Reference yield:

: 5176-27-2
N-tert-butyloxycarbonyl-pyrrole

: 5176-32-9
tert-butyl 1,2,3,4-tetrahydro-1,4-epiminonaphthalene-9-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / isoamyl nitrite / acetonitrile; CH₂Cl₂ / 2 h / Heating

2: 91 percent / H₂ / Pd/C / methanol / 6 h / 20 °C

With hydrogen; isopentyl nitrite; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja0658259