3-(4-(3-(4-methoxybenzyloxy)phenylamino)thieno[3,2-d]pyrimidin-6-yl)benzaldehyde

Base Information

Chemical Name:3-(4-(3-(4-methoxybenzyloxy)phenylamino)thieno[3,2-d]pyrimidin-6-yl)benzaldehyde
CAS No.:1228102-79-1
Molecular Formula:C₂₇H₂₁N₃O₃S
Molecular Weight:467.548
Hs Code.:

Synonyms:3-(4-(3-(4-methoxybenzyloxy)phenylamino)thieno[3,2-d]pyrimidin-6-yl)benzaldehyde

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Chemical Property of 3-(4-(3-(4-methoxybenzyloxy)phenylamino)thieno[3,2-d]pyrimidin-6-yl)benzaldehyde

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Technology Process of 3-(4-(3-(4-methoxybenzyloxy)phenylamino)thieno[3,2-d]pyrimidin-6-yl)benzaldehyde

There total 10 articles about 3-(4-(3-(4-methoxybenzyloxy)phenylamino)thieno[3,2-d]pyrimidin-6-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1228102-67-7
6-bromo-N-(3-(4-methoxybenzyloxy)phenyl)thieno[3,2-d]pyrimidin-4-amine

: 87199-16-4
3-Formylphenylboronic acid

: 1228102-79-1
3-(4-(3-(4-methoxybenzyloxy)phenylamino)thieno[3,2-d]pyrimidin-6-yl)benzaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 15h;

Reference yield:

: 1-(4-methoxybenzyloxy)-3-nitrobenzene

: 1228102-79-1
3-(4-(3-(4-methoxybenzyloxy)phenylamino)thieno[3,2-d]pyrimidin-6-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: iron; water / methanol / 15 h / Reflux

2: 1,2-dichloro-ethane; tert-butyl alcohol / 72 h / 85 °C / Sealed tube

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / N,N-dimethyl-formamide / 15 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; iron; sodium carbonate; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; tert-butyl alcohol; 3: |Suzuki Coupling;

Reference yield:

: 131770-85-9
3-[(4-methoxybenzyl)oxy]aniline

: 1228102-79-1
3-(4-(3-(4-methoxybenzyloxy)phenylamino)thieno[3,2-d]pyrimidin-6-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2-dichloro-ethane; tert-butyl alcohol / 72 h / 85 °C / Sealed tube

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / N,N-dimethyl-formamide / 15 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; tert-butyl alcohol; 2: |Suzuki Coupling;