C₃₁H₄₁N₅O₃Si

Base Information

Chemical Name:C₃₁H₄₁N₅O₃Si
CAS No.:1346246-43-2
Molecular Formula:C₃₁H₄₁N₅O₃Si
Molecular Weight:559.784
Hs Code.:

C<sub>31</sub>H<sub>41</sub>N<sub>5</sub>O<sub>3</sub>Si

Synonyms:C₃₁H₄₁N₅O₃Si

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Chemical Property of C₃₁H₄₁N₅O₃Si

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Technology Process of C₃₁H₄₁N₅O₃Si

There total 7 articles about C₃₁H₄₁N₅O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1346243-08-0
N-(cyclopropylmethyl)-N-(3,5-dimethoxyphenyl)-3-(1H-pyrazol-4-yl)quinoxaline-6-amine

: 86864-60-0
2-(tert-butyldimethylsilyloxy)ethyl bromide

: 1346246-43-2
C₃₁H₄₁N₅O₃Si

Guidance literature:: N-(cyclopropylmethyl)-N-(3,5-dimethoxyphenyl)-3-(1H-pyrazol-4-yl)quinoxaline-6-amine; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 1h;

2-(tert-butyldimethylsilyloxy)ethyl bromide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 4h;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1346246-43-2
C₃₁H₄₁N₅O₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: potassium phosphate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / 1,4-dioxane; water / 80 °C / Inert atmosphere

5.1: hydrogenchloride; water / 1,4-dioxane / 70 °C

5.2: Cooling with ice

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C

6.2: 4 h / 20 °C

With hydrogenchloride; potassium phosphate; water; sodium hydride; sodium t-butanolate; trichlorophosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; XPhos; In 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1346246-43-2
C₃₁H₄₁N₅O₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: potassium phosphate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / 1,4-dioxane; water / 80 °C / Inert atmosphere

5.1: hydrogenchloride; water / 1,4-dioxane / 70 °C

5.2: Cooling with ice

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C

6.2: 4 h / 20 °C

With hydrogenchloride; potassium phosphate; water; sodium hydride; sodium t-butanolate; trichlorophosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; XPhos; In 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;