methyl (2S,3R)-3-[(benzyloxycarbonyl)amino]-2-hydroxy-3-(4-methoxyphenyl)propionate

Base Information

Chemical Name:methyl (2S,3R)-3-[(benzyloxycarbonyl)amino]-2-hydroxy-3-(4-methoxyphenyl)propionate
CAS No.:305837-37-0
Molecular Formula:C₁₉H₂₁NO₆
Molecular Weight:359.379
Hs Code.:

Synonyms:methyl (2S,3R)-3-[(benzyloxycarbonyl)amino]-2-hydroxy-3-(4-methoxyphenyl)propionate

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Chemical Property of methyl (2S,3R)-3-[(benzyloxycarbonyl)amino]-2-hydroxy-3-(4-methoxyphenyl)propionate

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Technology Process of methyl (2S,3R)-3-[(benzyloxycarbonyl)amino]-2-hydroxy-3-(4-methoxyphenyl)propionate

There total 2 articles about methyl (2S,3R)-3-[(benzyloxycarbonyl)amino]-2-hydroxy-3-(4-methoxyphenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 621-84-1
O-benzyl carbamate

: 3901-07-3
3-(4-methoxy-phenyl)acrylic acid methyl ester

: 305837-37-0
methyl (2S,3R)-3-[(benzyloxycarbonyl)amino]-2-hydroxy-3-(4-methoxyphenyl)propionate

Guidance literature:: O-benzyl carbamate; With sodium hydroxide; tert-butylhypochlorite; 1,4-bis(9-O-dihydroquinidine)phthalazine; In propan-1-ol; water;

3-(4-methoxy-phenyl)acrylic acid methyl ester; With potassium dioxotetrahydroxoosmate(VI); In propan-1-ol; water; at 0 ℃; for 2h; Further stages.;
DOI:10.1021/ja0212314

Reference yield:

: 621-84-1
O-benzyl carbamate

: 3901-07-3
3-(4-methoxy-phenyl)acrylic acid methyl ester

: (2R,3S)-3-Benzyloxycarbonylamino-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid methyl ester

: 305837-37-0
methyl (2S,3R)-3-[(benzyloxycarbonyl)amino]-2-hydroxy-3-(4-methoxyphenyl)propionate

: (2S,3R)-2-Benzyloxycarbonylamino-3-hydroxy-3-(4-methoxy-phenyl)-propionic acid methyl ester

: (2R,3S)-2-Benzyloxycarbonylamino-3-hydroxy-3-(4-methoxy-phenyl)-propionic acid methyl ester

Guidance literature:: With sodium hydroxide; (DHQ)2AQN; tert-butylhypochlorite; K2; In propan-1-ol; water; for 1.5h; Yield given; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(98)00350-5