C₇₁H₈₆N₆O₁₁

Base Information

• Chemical Name: C₇₁H₈₆N₆O₁₁
• CAS No.: 1616282-97-3
• Molecular Formula: C₇₁H₈₆N₆O₁₁
• Molecular Weight: 1199.5
• Mol file: 1616282-97-3.mol

Synonyms:C₇₁H₈₆N₆O₁₁

Chemical Property of C₇₁H₈₆N₆O₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₇₁H₈₆N₆O₁₁

There total 4 articles about C₇₁H₈₆N₆O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

methyl galloate (99-24-1) + C21H27BrN2O2 (149474-78-2) → C71H86N6O11 (1616282-97-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ja5041573

Reference yield:

C21H28N2O3 (1575790-50-9) → C71H86N6O11 (1616282-97-3)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus tribromide / N,N-dimethyl-formamide; dichloromethane; tetrahydrofuran / 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

With phosphorus tribromide; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja5041573

Reference yield:

(E)-4-hydroxy-4′-methoxyazobenzene (103939-79-3) → C71H86N6O11 (1616282-97-3)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 14 h / 80 °C / Inert atmosphere

2: phosphorus tribromide / N,N-dimethyl-formamide; dichloromethane; tetrahydrofuran / 20 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

With phosphorus tribromide; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja5041573

upstream raw materials:

(E)-4-hydroxy-4′-methoxyazobenzene

C₂₁H₂₈N₂O₃

methyl galloate

C₂₁H₂₇BrN₂O₂

Downstream raw materials:

C₇₀H₈₆N₆O₁₀

C₇₀H₈₅ClN₆O₉

C₇₄H₉₁N₈O₉⁽¹⁺⁾*Cl^(1-)

Refernces