N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methylene)aniline oxide

Base Information

Chemical Name:N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methylene)aniline oxide
CAS No.:1613039-72-7
Molecular Formula:C₁₉H₁₁F₁₇N₄O
Molecular Weight:634.295
Hs Code.:

Synonyms:N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methylene)aniline oxide

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Chemical Property of N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methylene)aniline oxide

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Technology Process of N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methylene)aniline oxide

There total 4 articles about N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methylene)aniline oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1613039-93-2
N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methyl)aniline

: 1613039-72-7
N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methylene)aniline oxide

Guidance literature:: With selenium(IV) oxide; dihydrogen peroxide; In dichloromethane; water; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.04.052

Reference yield:

: 1424344-06-8
(1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-1H-(1,2,3)triazol-4-yl)methanol

: 1613039-72-7
N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methylene)aniline oxide

Guidance literature:: Multi-step reaction with 4 steps

1: Jones reagent / acetone / 0.58 h / 0 °C

2: acetonitrile / 6 h / 20 °C

3: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C

4: selenium(IV) oxide; dihydrogen peroxide / water; dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With selenium(IV) oxide; sodium tetrahydroborate; Jones reagent; dihydrogen peroxide; In methanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2014.04.052

Reference yield:

: 1424344-08-0
1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-1H-(1,2,3)triazole-4-carbaldehyde

: 1613039-72-7
N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methylene)aniline oxide

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 6 h / 20 °C

2: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C

3: selenium(IV) oxide; dihydrogen peroxide / water; dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With selenium(IV) oxide; sodium tetrahydroborate; dihydrogen peroxide; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.ejmech.2014.04.052